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A high-resolution Ca-43 solid-state NMR study of the calcium sites of hydroxyapatite

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<mark>Journal publication date</mark>1/02/2008
<mark>Journal</mark>Journal of the American Chemical Society
Issue number8
Volume130
Number of pages2
Pages (from-to)2412-2413
Publication StatusPublished
<mark>Original language</mark>English

Abstract

High resolution Ca-43 solid-state NMR studies of hydroxyapatite (Ca-10(PO4)(6)(OH2)) were performed at 14.1 T. The two crystallographically distinct calcium sites were unequivocally resolved by a triple-quantum magic angle spinning experiment, and the unambiguous assignment of the signals was possible using H-1-Ca-43 rotational echo double resonance and H-1-Ca-43 cross polarization magic angle spinning experiments.