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Boron-10 NMR: What extra information can it give about borate glasses?

Research output: Contribution to Journal/Magazine › Journal article › peer-review

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Standard

Boron-10 NMR: What extra information can it give about borate glasses? / Holland, D.; Feller, S.A.; Kemp, T.F. et al.
In: Physics and Chemistry of Glasses - European Journal of Glass Science and Technology Part B, Vol. 48, No. 1, 02.2007, p. 1-8.

Research output: Contribution to Journal/Magazine › Journal article › peer-review

Harvard

Holland, D, Feller, SA, Kemp, TF, Smith, ME, Howes, AP, Winslow, D & Kodama, M 2007, 'Boron-10 NMR: What extra information can it give about borate glasses?', Physics and Chemistry of Glasses - European Journal of Glass Science and Technology Part B, vol. 48, no. 1, pp. 1-8. <https://www.ingentaconnect.com/content/sgt/ejgst/2007/00000048/00000001/art00001>

APA

Holland, D., Feller, S. A., Kemp, T. F., Smith, M. E., Howes, A. P., Winslow, D., & Kodama, M. (2007). Boron-10 NMR: What extra information can it give about borate glasses? Physics and Chemistry of Glasses - European Journal of Glass Science and Technology Part B, 48(1), 1-8. https://www.ingentaconnect.com/content/sgt/ejgst/2007/00000048/00000001/art00001

Vancouver

Holland D, Feller SA, Kemp TF, Smith ME, Howes AP, Winslow D et al. Boron-10 NMR: What extra information can it give about borate glasses? Physics and Chemistry of Glasses - European Journal of Glass Science and Technology Part B. 2007 Feb;48(1):1-8.

Author

Holland, D. ; Feller, S.A. ; Kemp, T.F. et al. / Boron-10 NMR: What extra information can it give about borate glasses?. In: Physics and Chemistry of Glasses - European Journal of Glass Science and Technology Part B. 2007 ; Vol. 48, No. 1. pp. 1-8.

Bibtex

@article{0b18484323ac45278d899e7a7caab3b8,
title = "Boron-10 NMR: What extra information can it give about borate glasses?",
abstract = "We report the first 10B NMR experiments on borate glasses and related polycrystals using modern, fixed field, pulsed NMR in combination with a secondary field sweep coil. All six transitions from the I=3 nucleus could be observed. The spectra obtained have been compared with those simulated using third order perturbation theory and we have determined the quadrupole parameters for 10B in various systems with a precision which is more than an order of magnitude improved when compared with values reported to date from central transition 11B MAS NMR. The program used to simulate the data also allows a distribution of quadrupole parameters to be fitted for each distinct site, thus taking into account the distribution of environments for a given site in a glass.",
author = "D. Holland and S.A. Feller and T.F. Kemp and M.E. Smith and A.P. Howes and D. Winslow and M. Kodama",
year = "2007",
month = feb,
language = "English",
volume = "48",
pages = "1--8",
journal = "Physics and Chemistry of Glasses - European Journal of Glass Science and Technology Part B",
issn = "1753-3562",
publisher = "Society of Glass Technology",
number = "1",

}

RIS

TY - JOUR

T1 - Boron-10 NMR: What extra information can it give about borate glasses?

AU - Holland, D.

AU - Feller, S.A.

AU - Kemp, T.F.

AU - Smith, M.E.

AU - Howes, A.P.

AU - Winslow, D.

AU - Kodama, M.

PY - 2007/2

Y1 - 2007/2

N2 - We report the first 10B NMR experiments on borate glasses and related polycrystals using modern, fixed field, pulsed NMR in combination with a secondary field sweep coil. All six transitions from the I=3 nucleus could be observed. The spectra obtained have been compared with those simulated using third order perturbation theory and we have determined the quadrupole parameters for 10B in various systems with a precision which is more than an order of magnitude improved when compared with values reported to date from central transition 11B MAS NMR. The program used to simulate the data also allows a distribution of quadrupole parameters to be fitted for each distinct site, thus taking into account the distribution of environments for a given site in a glass.

AB - We report the first 10B NMR experiments on borate glasses and related polycrystals using modern, fixed field, pulsed NMR in combination with a secondary field sweep coil. All six transitions from the I=3 nucleus could be observed. The spectra obtained have been compared with those simulated using third order perturbation theory and we have determined the quadrupole parameters for 10B in various systems with a precision which is more than an order of magnitude improved when compared with values reported to date from central transition 11B MAS NMR. The program used to simulate the data also allows a distribution of quadrupole parameters to be fitted for each distinct site, thus taking into account the distribution of environments for a given site in a glass.

M3 - Journal article

VL - 48

SP - 1

EP - 8

JO - Physics and Chemistry of Glasses - European Journal of Glass Science and Technology Part B

JF - Physics and Chemistry of Glasses - European Journal of Glass Science and Technology Part B

SN - 1753-3562

IS - 1

ER -