Fourier transform infrared analysis of poly(ester-urethanes) at low temperature in-situ by using a newly constructed liquid nitrogen cooled sample stage

School of Engineering

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https://doi.org/10.1023/A:1018610719598
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Keywords

Absorption, Composition, Cooling, Fourier transform infrared spectroscopy, Hydrogen bonds, Infrared spectroscopy, Morphology, Structure (composition), Thermal effects, Hydrogen bonding, Liquid nitrogen sampling stage, Polyesterurethanes, Polyurethanes

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Fourier transform infrared analysis of poly(ester-urethanes) at low temperature in-situ by using a newly constructed liquid nitrogen cooled sample stage. / Rehman, I.; Barnardo, C.; Smith, R.
In: Journal of Materials Science, Vol. 32, No. 10, 1997, p. 2617-2621.

Research output: Contribution to Journal/Magazine › Journal article › peer-review

Bibtex

@article{503e897ddce04a0aa45ba567e91018db,

title = "Fourier transform infrared analysis of poly(ester-urethanes) at low temperature in-situ by using a newly constructed liquid nitrogen cooled sample stage",

abstract = "The design and use of an apparatus intended to cool samples for in-situ Fourier transform infrared (FTIR) spectroscopy study is described. Using liquid nitrogen as the cooling medium, a working sample temperature of - 165°C was achieved. The combination of the cooling stage and FTIR spectroscopy allowed us to study the hydrogen bonding in polyurethanes at very low temperatures in-situ. Experimental results in the N-H and carbonyl absorption regions as a function of temperature are compared.",

keywords = "Absorption, Composition, Cooling, Fourier transform infrared spectroscopy, Hydrogen bonds, Infrared spectroscopy, Morphology, Structure (composition), Thermal effects, Hydrogen bonding, Liquid nitrogen sampling stage, Polyesterurethanes, Polyurethanes",

author = "I. Rehman and C. Barnardo and R. Smith",

year = "1997",

doi = "10.1023/A:1018610719598",

language = "English",

volume = "32",

pages = "2617--2621",

journal = "Journal of Materials Science",

issn = "0022-2461",

publisher = "Springer Netherlands",

number = "10",

}

RIS

TY - JOUR

T1 - Fourier transform infrared analysis of poly(ester-urethanes) at low temperature in-situ by using a newly constructed liquid nitrogen cooled sample stage

AU - Rehman, I.

AU - Barnardo, C.

AU - Smith, R.

PY - 1997

Y1 - 1997

N2 - The design and use of an apparatus intended to cool samples for in-situ Fourier transform infrared (FTIR) spectroscopy study is described. Using liquid nitrogen as the cooling medium, a working sample temperature of - 165°C was achieved. The combination of the cooling stage and FTIR spectroscopy allowed us to study the hydrogen bonding in polyurethanes at very low temperatures in-situ. Experimental results in the N-H and carbonyl absorption regions as a function of temperature are compared.

AB - The design and use of an apparatus intended to cool samples for in-situ Fourier transform infrared (FTIR) spectroscopy study is described. Using liquid nitrogen as the cooling medium, a working sample temperature of - 165°C was achieved. The combination of the cooling stage and FTIR spectroscopy allowed us to study the hydrogen bonding in polyurethanes at very low temperatures in-situ. Experimental results in the N-H and carbonyl absorption regions as a function of temperature are compared.

KW - Absorption

KW - Composition

KW - Cooling

KW - Fourier transform infrared spectroscopy

KW - Hydrogen bonds

KW - Infrared spectroscopy

KW - Morphology

KW - Structure (composition)

KW - Thermal effects

KW - Hydrogen bonding

KW - Liquid nitrogen sampling stage

KW - Polyesterurethanes

KW - Polyurethanes

U2 - 10.1023/A:1018610719598

DO - 10.1023/A:1018610719598

M3 - Journal article

VL - 32

SP - 2617

EP - 2621

JO - Journal of Materials Science

JF - Journal of Materials Science

SN - 0022-2461

IS - 10

ER -

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