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Measure of microhardness, fracture toughness and flexural strength of N-vinylcaprolactam (NVC)-containing glass-ionomer dental cements

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Measure of microhardness, fracture toughness and flexural strength of N-vinylcaprolactam (NVC)-containing glass-ionomer dental cements. / Moshaverinia, A.; Brantley, W.A.; Chee, W.W.L.; Rohpour, N.; Ansari, S.; Zheng, F.; Heshmati, R.H.; Darr, J.A.; Schricker, S.R.; Rehman, I.U.

In: Dental Materials, Vol. 26, No. 12, 2010, p. 1137-1143.

Research output: Contribution to journalJournal articlepeer-review

Harvard

Moshaverinia, A, Brantley, WA, Chee, WWL, Rohpour, N, Ansari, S, Zheng, F, Heshmati, RH, Darr, JA, Schricker, SR & Rehman, IU 2010, 'Measure of microhardness, fracture toughness and flexural strength of N-vinylcaprolactam (NVC)-containing glass-ionomer dental cements', Dental Materials, vol. 26, no. 12, pp. 1137-1143. https://doi.org/10.1016/j.dental.2010.08.002

APA

Moshaverinia, A., Brantley, W. A., Chee, W. W. L., Rohpour, N., Ansari, S., Zheng, F., Heshmati, R. H., Darr, J. A., Schricker, S. R., & Rehman, I. U. (2010). Measure of microhardness, fracture toughness and flexural strength of N-vinylcaprolactam (NVC)-containing glass-ionomer dental cements. Dental Materials, 26(12), 1137-1143. https://doi.org/10.1016/j.dental.2010.08.002

Vancouver

Author

Moshaverinia, A. ; Brantley, W.A. ; Chee, W.W.L. ; Rohpour, N. ; Ansari, S. ; Zheng, F. ; Heshmati, R.H. ; Darr, J.A. ; Schricker, S.R. ; Rehman, I.U. / Measure of microhardness, fracture toughness and flexural strength of N-vinylcaprolactam (NVC)-containing glass-ionomer dental cements. In: Dental Materials. 2010 ; Vol. 26, No. 12. pp. 1137-1143.

Bibtex

@article{6400e049a6bd4734925dde4124b5dcef,
title = "Measure of microhardness, fracture toughness and flexural strength of N-vinylcaprolactam (NVC)-containing glass-ionomer dental cements",
abstract = "Objectives: To investigate the effects of N-vinylcaprolactam (NVC)-containing terpolymers on the fracture toughness, microhardness, and flexural strength of conventional glass-ionomer cements (GIC). Methods: The terpolymer of acrylic acid (AA)-itaconic acid (IA)-N-vinylcaprolactam (NVC) with 8:1:1 (AA:IA:NVC) molar ratio was synthesized by free radical polymerization and characterized using 1H NMR and FTIR. Experimental GIC samples were made from a 50% solution of the synthesized terpolymer with Fuji IX powder in a 3.6:1 P/L ratio. Specimens were mixed and fabricated at room temperature. Plane strain fracture toughness (KIc) was measured in accordance with ASTM Standard 399-05. Vickers hardness was determined using a microhardness tester. Flexural strength was measured using samples with dimensions of 2 mm × 2 mm × 20 mm. For all mechanical property tests, specimens were first conditioned in distilled water at 37 °C for 1 day or 1 week. Fracture toughness and flexural strength tests were conducted on a screw-driven universal testing machine using a crosshead speed of 0.5 mm/min. Values of mechanical properties for the experimental GIC were compared with the control group (Fuji IX GIC), using one-way ANOVA and the Tukey multiple range test at α = 0.05. Results: The NVC-modified GIC exhibited significantly higher fracture toughness compared to the commercially available Fuji IX GIC, along with higher mean values of flexural strength and Vickers hardness, which were not significantly different. Significance: It was concluded that NVC-containing polymers are capable of enhancing clinically relevant properties for GICs. This new modified glass-ionomer is a promising restorative dental material. {\textcopyright} 2010 Academy of Dental Materials.",
keywords = "Dental cements, Fracture toughness and flexural strength, Microhardness, N-vinylcaprolactam (NVC)-containing glass-ionomer, Acrylic acids, ASTM Standards, Control groups, Crosshead speed, Distilled water, Flexural strength, FTIR, Glass ionomer cement, Itaconic acid, Mean values, Microhardness tester, Molar ratio, One-way anova, Plane strain fracture toughness, Room temperature, Screw-driven, Universal testing machines, Bending strength, Carboxylic acids, Cements, Dental cement, Dental prostheses, Fracture, Fracture testing, Free radical polymerization, Free radicals, Glass, Intercalation, Mechanical properties, Organic acids, Polymers, Terpolymers, Vickers hardness, Fracture toughness, caprolactam, drug derivative, fuji IX, glass ionomer, poly N vinylcaprolactam, poly-N-vinylcaprolactam, polymer, article, chemistry, compressive strength, dental care, elasticity, hardness, materials testing, pliability, synthesis, tensile strength, Caprolactam, Compressive Strength, Dental Stress Analysis, Elasticity, Glass Ionomer Cements, Hardness, Materials Testing, Pliability, Tensile Strength",
author = "A. Moshaverinia and W.A. Brantley and W.W.L. Chee and N. Rohpour and S. Ansari and F. Zheng and R.H. Heshmati and J.A. Darr and S.R. Schricker and I.U. Rehman",
year = "2010",
doi = "10.1016/j.dental.2010.08.002",
language = "English",
volume = "26",
pages = "1137--1143",
journal = "Dental Materials",
issn = "0109-5641",
publisher = "Elsevier Inc.",
number = "12",

}

RIS

TY - JOUR

T1 - Measure of microhardness, fracture toughness and flexural strength of N-vinylcaprolactam (NVC)-containing glass-ionomer dental cements

AU - Moshaverinia, A.

AU - Brantley, W.A.

AU - Chee, W.W.L.

AU - Rohpour, N.

AU - Ansari, S.

AU - Zheng, F.

AU - Heshmati, R.H.

AU - Darr, J.A.

AU - Schricker, S.R.

AU - Rehman, I.U.

PY - 2010

Y1 - 2010

N2 - Objectives: To investigate the effects of N-vinylcaprolactam (NVC)-containing terpolymers on the fracture toughness, microhardness, and flexural strength of conventional glass-ionomer cements (GIC). Methods: The terpolymer of acrylic acid (AA)-itaconic acid (IA)-N-vinylcaprolactam (NVC) with 8:1:1 (AA:IA:NVC) molar ratio was synthesized by free radical polymerization and characterized using 1H NMR and FTIR. Experimental GIC samples were made from a 50% solution of the synthesized terpolymer with Fuji IX powder in a 3.6:1 P/L ratio. Specimens were mixed and fabricated at room temperature. Plane strain fracture toughness (KIc) was measured in accordance with ASTM Standard 399-05. Vickers hardness was determined using a microhardness tester. Flexural strength was measured using samples with dimensions of 2 mm × 2 mm × 20 mm. For all mechanical property tests, specimens were first conditioned in distilled water at 37 °C for 1 day or 1 week. Fracture toughness and flexural strength tests were conducted on a screw-driven universal testing machine using a crosshead speed of 0.5 mm/min. Values of mechanical properties for the experimental GIC were compared with the control group (Fuji IX GIC), using one-way ANOVA and the Tukey multiple range test at α = 0.05. Results: The NVC-modified GIC exhibited significantly higher fracture toughness compared to the commercially available Fuji IX GIC, along with higher mean values of flexural strength and Vickers hardness, which were not significantly different. Significance: It was concluded that NVC-containing polymers are capable of enhancing clinically relevant properties for GICs. This new modified glass-ionomer is a promising restorative dental material. © 2010 Academy of Dental Materials.

AB - Objectives: To investigate the effects of N-vinylcaprolactam (NVC)-containing terpolymers on the fracture toughness, microhardness, and flexural strength of conventional glass-ionomer cements (GIC). Methods: The terpolymer of acrylic acid (AA)-itaconic acid (IA)-N-vinylcaprolactam (NVC) with 8:1:1 (AA:IA:NVC) molar ratio was synthesized by free radical polymerization and characterized using 1H NMR and FTIR. Experimental GIC samples were made from a 50% solution of the synthesized terpolymer with Fuji IX powder in a 3.6:1 P/L ratio. Specimens were mixed and fabricated at room temperature. Plane strain fracture toughness (KIc) was measured in accordance with ASTM Standard 399-05. Vickers hardness was determined using a microhardness tester. Flexural strength was measured using samples with dimensions of 2 mm × 2 mm × 20 mm. For all mechanical property tests, specimens were first conditioned in distilled water at 37 °C for 1 day or 1 week. Fracture toughness and flexural strength tests were conducted on a screw-driven universal testing machine using a crosshead speed of 0.5 mm/min. Values of mechanical properties for the experimental GIC were compared with the control group (Fuji IX GIC), using one-way ANOVA and the Tukey multiple range test at α = 0.05. Results: The NVC-modified GIC exhibited significantly higher fracture toughness compared to the commercially available Fuji IX GIC, along with higher mean values of flexural strength and Vickers hardness, which were not significantly different. Significance: It was concluded that NVC-containing polymers are capable of enhancing clinically relevant properties for GICs. This new modified glass-ionomer is a promising restorative dental material. © 2010 Academy of Dental Materials.

KW - Dental cements

KW - Fracture toughness and flexural strength

KW - Microhardness

KW - N-vinylcaprolactam (NVC)-containing glass-ionomer

KW - Acrylic acids

KW - ASTM Standards

KW - Control groups

KW - Crosshead speed

KW - Distilled water

KW - Flexural strength

KW - FTIR

KW - Glass ionomer cement

KW - Itaconic acid

KW - Mean values

KW - Microhardness tester

KW - Molar ratio

KW - One-way anova

KW - Plane strain fracture toughness

KW - Room temperature

KW - Screw-driven

KW - Universal testing machines

KW - Bending strength

KW - Carboxylic acids

KW - Cements

KW - Dental cement

KW - Dental prostheses

KW - Fracture

KW - Fracture testing

KW - Free radical polymerization

KW - Free radicals

KW - Glass

KW - Intercalation

KW - Mechanical properties

KW - Organic acids

KW - Polymers

KW - Terpolymers

KW - Vickers hardness

KW - Fracture toughness

KW - caprolactam

KW - drug derivative

KW - fuji IX

KW - glass ionomer

KW - poly N vinylcaprolactam

KW - poly-N-vinylcaprolactam

KW - polymer

KW - article

KW - chemistry

KW - compressive strength

KW - dental care

KW - elasticity

KW - hardness

KW - materials testing

KW - pliability

KW - synthesis

KW - tensile strength

KW - Caprolactam

KW - Compressive Strength

KW - Dental Stress Analysis

KW - Elasticity

KW - Glass Ionomer Cements

KW - Hardness

KW - Materials Testing

KW - Pliability

KW - Tensile Strength

U2 - 10.1016/j.dental.2010.08.002

DO - 10.1016/j.dental.2010.08.002

M3 - Journal article

VL - 26

SP - 1137

EP - 1143

JO - Dental Materials

JF - Dental Materials

SN - 0109-5641

IS - 12

ER -