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Pushing the limits of sensitivity and resolution for natural abundance 43Ca NMR using ultra-high magnetic field (35.2 T)

Research output: Contribution to journalJournal article

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  • C. Bonhomme
  • X. Wang
  • I. Hung
  • Z. Gan
  • C. Gervais
  • C. Sassoye
  • J. Rimsza
  • J. Du
  • M.E. Smith
  • J.V. Hanna
  • S. Sarda
  • P. Gras
  • C. Combes
  • D. Laurencin
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<mark>Journal publication date</mark>7/09/2018
<mark>Journal</mark>Chemical Communications
Issue number69
Volume54
Number of pages4
Pages (from-to)9591-9594
Publication statusPublished
Early online date2/08/18
Original languageEnglish

Abstract

Natural abundance 43Ca solid state NMR experiments are reported for the first time at ultra-high magnetic field (35.2 T) on a series of Ca-(pyro)phosphate and Ca-oxalate materials, which are of biological relevance in relation to biomineralization processes and the formation of pathological calcifications. The significant gain in both sensitivity and resolution at 35.2 T leads to unprecedented insight into the structure of both crystalline and amorphous phases. © 2018 The Royal Society of Chemistry.

Bibliographic note

© Royal Society of Chemistry 2018