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Research

Professor Mark Smith

Visiting Professor, Professor of Solid State NMR

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  1. Published

    (33)S MAS NMR of a disordered sulfur-doped silicate: signal enhancement via RAPT, QCPMG and adiabatic pulses

    O'Dell, L. A., Klimm, K., Freitas, J. C. C., Kohn, S. C. & Smith, M. E., 1/02/2009, In: Applied Magnetic Resonance. 35, 2, p. 247-259 13 p.

    Research output: Contribution to Journal/Magazine › Journal article › peer-review

  2. Published

    (59)Co NMR study of the allotropic phase transformation in small ferromagnetic cobalt particles

    Speight, R. J., Wong, A., Ellis, P., Bishop, P. T., Hyde, T. I., Bastow, T. J. & Smith, M. E., 1/02/2009, In: Physical review B. 79, 5, 8 p., 054102.

    Research output: Contribution to Journal/Magazine › Journal article › peer-review

  3. Published

    17O and 15N Solid State NMR Studies on Ligand-Assisted Templating and Oxygen Coordination in the Walls of Mesoporous Nb, Ta and Ti Oxides

    Rao, Y., Kemp, T. F., Trudeau, M., Smith, M. E. & Antonelli, D. M., 19/11/2008, In: Journal of the American Chemical Society. 130, 46, p. 15726-15731 6 p.

    Research output: Contribution to Journal/Magazine › Journal article › peer-review

  4. Published

    1H and 13C solution- and solid-state NMR investigation into wax products from the Fischer-Tropsch process

    Speight, R. J., Rourke, J. P., Wong, A., Barrow, N. S., Ellis, P. R., Bishop, P. T. & Smith, M. E., 2011, In: Solid State Nuclear Magnetic Resonance. 39, 3-4, p. 58-64 7 p.

    Research output: Contribution to Journal/Magazine › Journal article › peer-review

  5. Published

    87Sr, 119Sn, 127I Single and {1H/19F}-Double Resonance Solid-State NMR Experiments: Application to Inorganic Materials and Nanobuilding Blocks

    Laurencin, D., Ribot, F., Gervais, C., Wright, A. J., Baker, A. R., Campayo, L., Hanna, J. V., Iuga, D., Smith, M. E., Nedelec, J-M., Renaudin, G. & Bonhomme, C., 16/09/2016, In: ChemistrySelect. 1, 15, p. 4509-4519 11 p.

    Research output: Contribution to Journal/Magazine › Journal article › peer-review

  6. Published

    A 93Nb Solid-State NMR and Density Functional Theory Study of Four- and Six-Coordinate Niobate Systems

    Hanna, J. V., Pike, K. J., Charpentier, T., Kemp, T. F., Smith, M. E., Lucier, B. E. G., Schurko, R. W. & Cahill, L. S., 8/03/2010, In: Chemistry - A European Journal. 16, 10, p. 3222-3239 18 p.

    Research output: Contribution to Journal/Magazine › Journal article › peer-review

  7. Published

    A Al-27 MAS NMR study of a sol-gel produced alumina: Identification of the NMR parameters of the theta-Al2O3 transition alumina phase

    O'Dell, L. A., Savin, S. L. P., Chadwick, A. V. & Smith, M. E., 1/07/2007, In: Solid State Nuclear Magnetic Resonance. 31, 4, p. 169-173 5 p.

    Research output: Contribution to Journal/Magazine › Journal article › peer-review

  8. Published

    A Co-59 NMR study to observe the effects of ball milling on small ferromagnetic cobalt particles

    Speight, R. J., Wong, A., Ellis, P., Hyde, T., Bishop, P. T. & Smith, M. E., 1/04/2009, In: Solid State Nuclear Magnetic Resonance. 35, 2, p. 67-73 7 p.

    Research output: Contribution to Journal/Magazine › Journal article › peer-review

  9. Published

    A Combined Mg-25 Solid-State NMR and Ab Initio DFT Approach to Probe the Local Structural Differences in Magnesium Acetate Phases Mg(CH3COO)(2)center dot nH(2)O (n=0,1,4)

    Seymour, V. R., Day, S. P., Scholz, G., Scheurell, K., Iuga, D., Griffin, J. M., Kemnitz, E., Hanna, J. V. & Smith, M. E., 17/07/2018, In: ChemPhysChem. 19, 14, p. 1722-1732 11 p.

    Research output: Contribution to Journal/Magazine › Journal article › peer-review

  10. Published

    A comparative study of the structure of sodium borophosphates made by sol–gel and melt-quench methods

    Qiu, D., Martin, R. A., Knowles, J. C., Smith, M. E. & Newport, R. J., 15/03/2010, In: Journal of Non-Crystalline Solids. 356, 9-10, p. 490-494 5 p.

    Research output: Contribution to Journal/Magazine › Journal article › peer-review

  11. Published

    A first-principles computational O-17 NMR investigation of metal ion-oxygen interactions in carboxylate oxygens of alkali oxalates

    Wong, A., Thurgood, G., Dupree, R. & Smith, M. E., 1/08/2007, In: Chemical Physics Letters. 337, 1-3, p. 144-150 7 p.

    Research output: Contribution to Journal/Magazine › Journal article › peer-review

  12. Published

    A high-energy X-ray diffraction, P-31 and B-11 solid-state NMR study of the structure of aged sodium borophosphate glasses

    Qiu, D., Guerry, P., Ahmed, I., Pickup, D. M., Carta, D., Knowles, J. C., Smith, M. E. & Newport, R. J., 1/10/2008, In: Materials Chemistry and Physics. 111, 2-3, p. 455-462 8 p.

    Research output: Contribution to Journal/Magazine › Journal article › peer-review

  13. Published

    A high-resolution Ca-43 solid-state NMR study of the calcium sites of hydroxyapatite

    Laurencin, D., Wong, A., Hanna, J. V., Dupree, R. & Smith, M. E., 1/02/2008, In: Journal of the American Chemical Society. 130, 8, p. 2412-2413 2 p.

    Research output: Contribution to Journal/Magazine › Journal article › peer-review

  14. Published

    A High-Resolution NMR Study of the La-Si-Al-O-N System

    Dupree, R., Lewis, M. H. & Smith, M. E., 1989, In: Journal of the American Chemical Society. 111, 14, p. 5125-5132 8 p.

    Research output: Contribution to Journal/Magazine › Journal article › peer-review

  15. Published

    A multinuclear solid state NMR spectroscopic study of the structural evolution of disordered calcium silicate sol–gel biomaterials

    Lin, Z., Jones, J. R., Hanna, J. V. & Smith, M. E., 28/01/2015, In: Physical Chemistry Chemical Physics. 17, 4, p. 2540-2549 10 p.

    Research output: Contribution to Journal/Magazine › Journal article › peer-review

  16. Published

    A multinuclear solid state NMR, density functional theory and X-Ray diffraction study of hydrogen bonding in Group I hydrogen dibenzoates

    Rees, G. J., Day, S. P., Lari, A., Howes, A. P., Iuga, D., Pitak, M. B., Coles, S. J., Threlfall, T. L., Light, M. E., Smith, M. E., Quigley, D., Wallis, J. D. & Hanna, J. V., 21/11/2013, In: CrystEngComm. 15, 43, p. 8823-8839 17 p.

    Research output: Contribution to Journal/Magazine › Journal article › peer-review

  17. Published

    A multiple-field Na-23 NMR study of sodium species in porous carbons

    Freitas, J. C. C., Schettino, M. A., Emmerich, F. G., Wong, A. & Smith, M. E., 1/12/2007, In: Solid State Nuclear Magnetic Resonance. 32, 4, p. 109-117 9 p.

    Research output: Contribution to Journal/Magazine › Journal article › peer-review

  18. Published

    A multispectroscopic structural study of lead silicate glasses over an extended range of compositions

    Feller, S., Lodden, G., Riley, A., Edwards, T., Croskrey, J., Schue, A., Liss, D., Stentz, D., Blair, S., Kelley, M., Smith, G., Singleton, S., Affatigato, M., Holland, D., Smith, M. E., Kamitsos, E. I., Varsamis, C. P. E. & Ioannou, E., 1/03/2010, In: Journal of Non-Crystalline Solids. 356, 6-8, p. 304-313 10 p.

    Research output: Contribution to Journal/Magazine › Journal article › peer-review

  19. Published

    A natural abundance Se-77 solid-state NMR study of inorganic compounds

    Kemp, T. F., Wong, A., Smith, M. E., Bishop, P. T. & Carthey, N., 1/11/2008, In: Solid State Nuclear Magnetic Resonance. 34, 4, p. 224-227 4 p.

    Research output: Contribution to Journal/Magazine › Journal article › peer-review

  20. Published

    A potential novel rapid screening NMR approach to boundary film formation at solid interfaces in contact with ionic liquids

    Forsyth, M., Kemp, T. F., Howlett, P. C., Sun, J. & Smith, M. E., 1/09/2008, In: The Journal of Physical Chemistry C. 112, 36, p. 13801-13804 4 p.

    Research output: Contribution to Journal/Magazine › Journal article › peer-review

  21. Published

    A Si-29 MAS NMR study of silicate glasses with a high lithium content

    Larson, C., Doerr, J., Affatigato, M., Feller, S., Holland, D. & Smith, M. E., 2006, In: Journal of Physics: Condensed Matter. 18, 49, p. 11323-11331 9 p.

    Research output: Contribution to Journal/Magazine › Journal article › peer-review

  22. Published

    A soft-chemistry approach to the synthesis of amorphous calcium ortho/pyrophosphate biomaterials of tunable composition

    Mayen, L., Jensen, N. D., Laurencin, D., Marsan, O., Bonhomme, C., Gervais, C., Smith, M. E., Coelho, C., Laurent, G., Trebosc, J., Gan, Z., Chen, K., Rey, C., Combes, C. & Soulié, J., 28/02/2020, In: Acta Biomaterialia. 103, p. 333-345 13 p.

    Research output: Contribution to Journal/Magazine › Journal article › peer-review

  23. Published

    A solid-state NMR study of lead and vanadium substitution into hydroxyapatite

    Pizzala, H., Caldarelli, S., Eon, J-G., Rossi, A. M., Laurencin, D. & Smith, M. E., 1/04/2009, In: Journal of the American Chemical Society. 131, 14, p. 5145-5152 8 p.

    Research output: Contribution to Journal/Magazine › Journal article › peer-review

  24. Published

    A spectrometer designed for 6.7 and 14.1 T DNP-enhanced solid-state MAS NMR using quasi-optical microwave transmission

    Pike, K. J., Kemp, T. F., Takahashi, H., Day, R., Howes, A. P., Kryukov, E. V., MacDonald, J. F., Collis, A. E. C., Bolton, D. R., Wylde, R. J., Orwick, M., Kosuga, K., Clark, A. J., Idehara, T., Watts, A., Smith, G. M., Newton, M. E., Dupree, R. & Smith, M. E., 02/2012, In: Journal of Magnetic Resonance. 215, p. 1-9 9 p.

    Research output: Contribution to Journal/Magazine › Journal article › peer-review

  25. Published

    A structural investigation of the alkali metal site distribution within bioactive glass using neutron diffraction and multinuclear solid state NMR

    Martin, R. A., Twyman, H. L., Rees, G. J., Smith, J. M., Barney, E. R., Smith, M. E., Hanna, J. V. & Newport, R. J., 15/08/2012, In: Physical Chemistry Chemical Physics. 14, 35, p. 12105-12113 9 p.

    Research output: Contribution to Journal/Magazine › Journal article › peer-review

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