13C NMR spectroscopy of keratan sulphates : assignments for the reduced form of a repeat unit tetrasaccharide derived from keratan sulphate by a keratanase digestion and partial assignments for two fucosylated pentasaccharides.

Research output: Contribution to Journal/Magazine › Journal article › peer-review

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13C NMR spectroscopy of keratan sulphates : assignments for the reduced form of a repeat unit tetrasaccharide derived from keratan sulphate by a keratanase digestion and partial assignments for two fucosylated pentasaccharides. / Huckerby, Thomas; Dickerson, John; Tai, G.H. et al.
In: Magnetic Resonance in Chemistry, Vol. 31, No. 4, 1993, p. 394-398.

Research output: Contribution to Journal/Magazine › Journal article › peer-review

Harvard

Huckerby, T, Dickerson, J, Tai, GH, Lauder, R, Brown, G & Nieduszynski, I 1993, '13C NMR spectroscopy of keratan sulphates : assignments for the reduced form of a repeat unit tetrasaccharide derived from keratan sulphate by a keratanase digestion and partial assignments for two fucosylated pentasaccharides.', Magnetic Resonance in Chemistry, vol. 31, no. 4, pp. 394-398. https://doi.org/10.1002/mrc.1260310416

APA

Huckerby, T., Dickerson, J., Tai, G. H., Lauder, R., Brown, G., & Nieduszynski, I. (1993). 13C NMR spectroscopy of keratan sulphates : assignments for the reduced form of a repeat unit tetrasaccharide derived from keratan sulphate by a keratanase digestion and partial assignments for two fucosylated pentasaccharides. Magnetic Resonance in Chemistry, 31(4), 394-398. https://doi.org/10.1002/mrc.1260310416

Vancouver

Huckerby T, Dickerson J, Tai GH, Lauder R, Brown G, Nieduszynski I. 13C NMR spectroscopy of keratan sulphates : assignments for the reduced form of a repeat unit tetrasaccharide derived from keratan sulphate by a keratanase digestion and partial assignments for two fucosylated pentasaccharides. Magnetic Resonance in Chemistry. 1993;31(4):394-398. doi: 10.1002/mrc.1260310416

Author

Huckerby, Thomas ; Dickerson, John ; Tai, G.H. et al. / 13C NMR spectroscopy of keratan sulphates : assignments for the reduced form of a repeat unit tetrasaccharide derived from keratan sulphate by a keratanase digestion and partial assignments for two fucosylated pentasaccharides. In: Magnetic Resonance in Chemistry. 1993 ; Vol. 31, No. 4. pp. 394-398.

Bibtex

@article{cf4ee0d0d1b44e2dba17834abda43e6b,

title = "13C NMR spectroscopy of keratan sulphates : assignments for the reduced form of a repeat unit tetrasaccharide derived from keratan sulphate by a keratanase digestion and partial assignments for two fucosylated pentasaccharides.",

abstract = "A full assignment of the 60°C 13C NMR spectrum for the reduced form of a repeat unit β-linked tetrasaccharide derived by keratanase digestion from keratan sulphate, GlcNAc(6SO4)β1–3Gal(6SO4)β1–4GlcNAc(6SO4)β1–3-Gal-ol, was achieved via two-dimensional C/H correlation and 1H COSY experiments, and a complete first-order analysis of the 600 MHz proton spectrum. Partial 13C assignments for two fucosylated keratan sulphate pentasc-charides derived using hydrazinolysis and nitrous acid treatment are discussed.",

keywords = "Keratan sulphate, 13C NMR, C/H correlation, Oligosaccharides, Structural assignment",

author = "Thomas Huckerby and John Dickerson and G.H. Tai and Robert Lauder and Gavin Brown and Ian Nieduszynski",

year = "1993",

doi = "10.1002/mrc.1260310416",

language = "English",

volume = "31",

pages = "394--398",

journal = "Magnetic Resonance in Chemistry",

issn = "1097-458X",

publisher = "John Wiley and Sons Ltd",

number = "4",

}

RIS

TY - JOUR

T1 - 13C NMR spectroscopy of keratan sulphates : assignments for the reduced form of a repeat unit tetrasaccharide derived from keratan sulphate by a keratanase digestion and partial assignments for two fucosylated pentasaccharides.

AU - Huckerby, Thomas

AU - Dickerson, John

AU - Tai, G.H.

AU - Lauder, Robert

AU - Brown, Gavin

AU - Nieduszynski, Ian

PY - 1993

Y1 - 1993

N2 - A full assignment of the 60°C 13C NMR spectrum for the reduced form of a repeat unit β-linked tetrasaccharide derived by keratanase digestion from keratan sulphate, GlcNAc(6SO4)β1–3Gal(6SO4)β1–4GlcNAc(6SO4)β1–3-Gal-ol, was achieved via two-dimensional C/H correlation and 1H COSY experiments, and a complete first-order analysis of the 600 MHz proton spectrum. Partial 13C assignments for two fucosylated keratan sulphate pentasc-charides derived using hydrazinolysis and nitrous acid treatment are discussed.

AB - A full assignment of the 60°C 13C NMR spectrum for the reduced form of a repeat unit β-linked tetrasaccharide derived by keratanase digestion from keratan sulphate, GlcNAc(6SO4)β1–3Gal(6SO4)β1–4GlcNAc(6SO4)β1–3-Gal-ol, was achieved via two-dimensional C/H correlation and 1H COSY experiments, and a complete first-order analysis of the 600 MHz proton spectrum. Partial 13C assignments for two fucosylated keratan sulphate pentasc-charides derived using hydrazinolysis and nitrous acid treatment are discussed.

KW - Keratan sulphate

KW - 13C NMR

KW - C/H correlation

KW - Oligosaccharides

KW - Structural assignment

U2 - 10.1002/mrc.1260310416

DO - 10.1002/mrc.1260310416

M3 - Journal article

VL - 31

SP - 394

EP - 398

JO - Magnetic Resonance in Chemistry

JF - Magnetic Resonance in Chemistry

SN - 1097-458X

IS - 4

ER -

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