Research output: Contribution to Journal/Magazine › Journal article › peer-review
Research output: Contribution to Journal/Magazine › Journal article › peer-review
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TY - JOUR
T1 - A high-resolution Ca-43 solid-state NMR study of the calcium sites of hydroxyapatite
AU - Laurencin, Danielle
AU - Wong, Alan
AU - Hanna, John V.
AU - Dupree, Ray
AU - Smith, Mark E.
PY - 2008/2/1
Y1 - 2008/2/1
N2 - High resolution Ca-43 solid-state NMR studies of hydroxyapatite (Ca-10(PO4)(6)(OH2)) were performed at 14.1 T. The two crystallographically distinct calcium sites were unequivocally resolved by a triple-quantum magic angle spinning experiment, and the unambiguous assignment of the signals was possible using H-1-Ca-43 rotational echo double resonance and H-1-Ca-43 cross polarization magic angle spinning experiments.
AB - High resolution Ca-43 solid-state NMR studies of hydroxyapatite (Ca-10(PO4)(6)(OH2)) were performed at 14.1 T. The two crystallographically distinct calcium sites were unequivocally resolved by a triple-quantum magic angle spinning experiment, and the unambiguous assignment of the signals was possible using H-1-Ca-43 rotational echo double resonance and H-1-Ca-43 cross polarization magic angle spinning experiments.
UR - http://www.scopus.com/inward/record.url?scp=39749099237&partnerID=8YFLogxK
U2 - 10.1021/ja710557t
DO - 10.1021/ja710557t
M3 - Journal article
VL - 130
SP - 2412
EP - 2413
JO - Journal of the American Chemical Society
JF - Journal of the American Chemical Society
SN - 1520-5126
IS - 8
ER -