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Accelerated acquisition in pure-shift spectra based on prior knowledge from 1H NMR

Research output: Contribution to Journal/Magazine › Journal article › peer-review

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Accelerated acquisition in pure-shift spectra based on prior knowledge from 1H NMR. / Shchukina, Alexandra; Kaźmierczak, Magdalena; Kasprzak, Paweł et al.
In: Chemical Communications, Vol. 55, No. 64, 18.07.2019, p. 9563-9566.

Research output: Contribution to Journal/Magazine › Journal article › peer-review

Harvard

Shchukina, A, Kaźmierczak, M, Kasprzak, P, Davy, M, Akien, G, Butts, C & Kazimierczuk, K 2019, 'Accelerated acquisition in pure-shift spectra based on prior knowledge from 1H NMR', Chemical Communications, vol. 55, no. 64, pp. 9563-9566. https://doi.org/10.1039/C9CC05222D

APA

Shchukina, A., Kaźmierczak, M., Kasprzak, P., Davy, M., Akien, G., Butts, C., & Kazimierczuk, K. (2019). Accelerated acquisition in pure-shift spectra based on prior knowledge from 1H NMR. Chemical Communications, 55(64), 9563-9566. https://doi.org/10.1039/C9CC05222D

Vancouver

Shchukina A, Kaźmierczak M, Kasprzak P, Davy M, Akien G, Butts C et al. Accelerated acquisition in pure-shift spectra based on prior knowledge from 1H NMR. Chemical Communications. 2019 Jul 18;55(64):9563-9566. doi: 10.1039/C9CC05222D

Author

Shchukina, Alexandra ; Kaźmierczak, Magdalena ; Kasprzak, Paweł et al. / Accelerated acquisition in pure-shift spectra based on prior knowledge from 1H NMR. In: Chemical Communications. 2019 ; Vol. 55, No. 64. pp. 9563-9566.

Bibtex

@article{ae5f02c8073d404295bcddc5de84cda6,
title = "Accelerated acquisition in pure-shift spectra based on prior knowledge from 1H NMR",
abstract = "Pure-shift NMR enhances the spectral resolution, but the optimal resolutions can only be obtained at the cost of the acquisition time. We propose to accelerate the acquisition using optimised {\textquoteright}burst{\textquoteright} non-uniform sampling schemes[I. E. Ndukwe, A. Shchukina, K. Kazimierczuk, C. P. Butts,ChemComm, 2016, 52, 12769] and then reconstructing the undersampled signal mathematically. Here, we focus on the reliability of this reconstruction depending on the sampling scheme and present a workflow for the sampling optimization. It is ready to be implemented in routine measurements and yields a great improvement of the reconstruction in challenging cases.",
author = "Alexandra Shchukina and Magdalena Ka{\'z}mierczak and Pawe{\l} Kasprzak and Matthew Davy and Geoffrey Akien and Craig Butts and Krzysztof Kazimierczuk",
year = "2019",
month = jul,
day = "18",
doi = "10.1039/C9CC05222D",
language = "English",
volume = "55",
pages = "9563--9566",
journal = "Chemical Communications",
issn = "1359-7345",
publisher = "Royal Society of Chemistry",
number = "64",

}

RIS

TY - JOUR

T1 - Accelerated acquisition in pure-shift spectra based on prior knowledge from 1H NMR

AU - Shchukina, Alexandra

AU - Kaźmierczak, Magdalena

AU - Kasprzak, Paweł

AU - Davy, Matthew

AU - Akien, Geoffrey

AU - Butts, Craig

AU - Kazimierczuk, Krzysztof

PY - 2019/7/18

Y1 - 2019/7/18

N2 - Pure-shift NMR enhances the spectral resolution, but the optimal resolutions can only be obtained at the cost of the acquisition time. We propose to accelerate the acquisition using optimised ’burst’ non-uniform sampling schemes[I. E. Ndukwe, A. Shchukina, K. Kazimierczuk, C. P. Butts,ChemComm, 2016, 52, 12769] and then reconstructing the undersampled signal mathematically. Here, we focus on the reliability of this reconstruction depending on the sampling scheme and present a workflow for the sampling optimization. It is ready to be implemented in routine measurements and yields a great improvement of the reconstruction in challenging cases.

AB - Pure-shift NMR enhances the spectral resolution, but the optimal resolutions can only be obtained at the cost of the acquisition time. We propose to accelerate the acquisition using optimised ’burst’ non-uniform sampling schemes[I. E. Ndukwe, A. Shchukina, K. Kazimierczuk, C. P. Butts,ChemComm, 2016, 52, 12769] and then reconstructing the undersampled signal mathematically. Here, we focus on the reliability of this reconstruction depending on the sampling scheme and present a workflow for the sampling optimization. It is ready to be implemented in routine measurements and yields a great improvement of the reconstruction in challenging cases.

U2 - 10.1039/C9CC05222D

DO - 10.1039/C9CC05222D

M3 - Journal article

VL - 55

SP - 9563

EP - 9566

JO - Chemical Communications

JF - Chemical Communications

SN - 1359-7345

IS - 64

ER -