Analysis of in vitro reaction layers formed on Bioglass® using thin- film X-ray diffraction and ATR-FTIR microspectroscopy

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Analysis of in vitro reaction layers formed on Bioglass® using thin- film X-ray diffraction and ATR-FTIR microspectroscopy. / Rehman, I.; Knowles, J.C.; Bonfield, W.
In: Journal of Biomedical Materials Research Part A, Vol. 41, No. 1, 1998, p. 162-166.

Research output: Contribution to Journal/Magazine › Journal article › peer-review

Harvard

Rehman, I, Knowles, JC & Bonfield, W 1998, 'Analysis of in vitro reaction layers formed on Bioglass® using thin- film X-ray diffraction and ATR-FTIR microspectroscopy', Journal of Biomedical Materials Research Part A, vol. 41, no. 1, pp. 162-166. https://doi.org/10.1002/(SICI)1097-4636(199807)41:1<162::AID-JBM19>3.0.CO;2-P

APA

Rehman, I., Knowles, J. C., & Bonfield, W. (1998). Analysis of in vitro reaction layers formed on Bioglass® using thin- film X-ray diffraction and ATR-FTIR microspectroscopy. Journal of Biomedical Materials Research Part A, 41(1), 162-166. https://doi.org/10.1002/(SICI)1097-4636(199807)41:1<162::AID-JBM19>3.0.CO;2-P

Vancouver

Rehman I, Knowles JC, Bonfield W. Analysis of in vitro reaction layers formed on Bioglass® using thin- film X-ray diffraction and ATR-FTIR microspectroscopy. Journal of Biomedical Materials Research Part A. 1998;41(1):162-166. doi: 10.1002/(SICI)1097-4636(199807)41:1<162::AID-JBM19>3.0.CO;2-P

Author

Rehman, I. ; Knowles, J.C. ; Bonfield, W. / Analysis of in vitro reaction layers formed on Bioglass® using thin- film X-ray diffraction and ATR-FTIR microspectroscopy. In: Journal of Biomedical Materials Research Part A. 1998 ; Vol. 41, No. 1. pp. 162-166.

Bibtex

@article{323f605ffa7c44d2befe627eaebd2716,

title = "Analysis of in vitro reaction layers formed on Bioglass{\textregistered} using thin- film X-ray diffraction and ATR-FTIR microspectroscopy",

abstract = "Fourier transform infrared spectroscopy and thin-film X-ray diffraction (TF-XRD) techniques were used to analyze the inorganic carbonate apatite (CA) layer developed on a bioactive glass (45S5 type Bioglass{\textregistered}) in an in vitro environment. The C-O and P-O vibrational modes appeared on the bioactive glass surface following immersion in the simulated body fluid solution. Initially, the C-O and P-O peaks increased with immersion time as crystallization of CA phase progressed. The TF-XRD confirmed that the deposited layer was apatite, crystallographically. Furthermore, evidence of preferred orientation in the 001 direction was seen, indicated by very strong 002 reflection. With time, the crystal growth became more random and the intensity of the 002 reflection decreased. Fourier transform infrared spectroscopy and thin-film X-ray diffraction (TF-XRD) techniques were used to analyze the inorganic carbonate apatite (CA) layer developed on a bioactive glass (45S5 type BioglassR) in an in vitro environment. The C-O and P-O vibrational modes appeared on the bioactive glass surface following immersion in the simulated body fluid solution. Initially, the C-O and P-O peaks increased with immersion time as crystallization of CA phase progressed. The TF-XRD confirmed that the deposited layer was apatite, crystallographically. Furthermore, evidence of preferred orientation in the 001 direction was seen, indicated by very strong 002 reflection. With time, the crystal growth became more random and the intensity of the 002 reflection decreased.",

keywords = "Bioactive glasses, FTIR spectroscopy, In vitro, Simulated body fluid, X-ray diffraction, Body fluids, Crystallization, Fourier transform infrared spectroscopy, Glass, Phosphates, Thin films, X ray diffraction analysis, Thin film X ray diffraction, Bone cement, article, chemical analysis, crystal structure, crystallization, immersion, infrared spectroscopy, vibration, X ray diffraction, Biocompatible Materials, Spectroscopy, Fourier Transform Infrared, X-Ray Diffraction",

author = "I. Rehman and J.C. Knowles and W. Bonfield",

year = "1998",

doi = "10.1002/(SICI)1097-4636(199807)41:1<162::AID-JBM19>3.0.CO;2-P",

language = "English",

volume = "41",

pages = "162--166",

journal = "Journal of Biomedical Materials Research Part A",

issn = "0021-9304",

publisher = "John Wiley and Sons Inc.",

number = "1",

}

RIS

TY - JOUR

T1 - Analysis of in vitro reaction layers formed on Bioglass® using thin- film X-ray diffraction and ATR-FTIR microspectroscopy

AU - Rehman, I.

AU - Knowles, J.C.

AU - Bonfield, W.

PY - 1998

Y1 - 1998

N2 - Fourier transform infrared spectroscopy and thin-film X-ray diffraction (TF-XRD) techniques were used to analyze the inorganic carbonate apatite (CA) layer developed on a bioactive glass (45S5 type Bioglass®) in an in vitro environment. The C-O and P-O vibrational modes appeared on the bioactive glass surface following immersion in the simulated body fluid solution. Initially, the C-O and P-O peaks increased with immersion time as crystallization of CA phase progressed. The TF-XRD confirmed that the deposited layer was apatite, crystallographically. Furthermore, evidence of preferred orientation in the 001 direction was seen, indicated by very strong 002 reflection. With time, the crystal growth became more random and the intensity of the 002 reflection decreased. Fourier transform infrared spectroscopy and thin-film X-ray diffraction (TF-XRD) techniques were used to analyze the inorganic carbonate apatite (CA) layer developed on a bioactive glass (45S5 type BioglassR) in an in vitro environment. The C-O and P-O vibrational modes appeared on the bioactive glass surface following immersion in the simulated body fluid solution. Initially, the C-O and P-O peaks increased with immersion time as crystallization of CA phase progressed. The TF-XRD confirmed that the deposited layer was apatite, crystallographically. Furthermore, evidence of preferred orientation in the 001 direction was seen, indicated by very strong 002 reflection. With time, the crystal growth became more random and the intensity of the 002 reflection decreased.

AB - Fourier transform infrared spectroscopy and thin-film X-ray diffraction (TF-XRD) techniques were used to analyze the inorganic carbonate apatite (CA) layer developed on a bioactive glass (45S5 type Bioglass®) in an in vitro environment. The C-O and P-O vibrational modes appeared on the bioactive glass surface following immersion in the simulated body fluid solution. Initially, the C-O and P-O peaks increased with immersion time as crystallization of CA phase progressed. The TF-XRD confirmed that the deposited layer was apatite, crystallographically. Furthermore, evidence of preferred orientation in the 001 direction was seen, indicated by very strong 002 reflection. With time, the crystal growth became more random and the intensity of the 002 reflection decreased. Fourier transform infrared spectroscopy and thin-film X-ray diffraction (TF-XRD) techniques were used to analyze the inorganic carbonate apatite (CA) layer developed on a bioactive glass (45S5 type BioglassR) in an in vitro environment. The C-O and P-O vibrational modes appeared on the bioactive glass surface following immersion in the simulated body fluid solution. Initially, the C-O and P-O peaks increased with immersion time as crystallization of CA phase progressed. The TF-XRD confirmed that the deposited layer was apatite, crystallographically. Furthermore, evidence of preferred orientation in the 001 direction was seen, indicated by very strong 002 reflection. With time, the crystal growth became more random and the intensity of the 002 reflection decreased.

KW - Bioactive glasses

KW - FTIR spectroscopy

KW - In vitro

KW - Simulated body fluid

KW - X-ray diffraction

KW - Body fluids

KW - Crystallization

KW - Fourier transform infrared spectroscopy

KW - Glass

KW - Phosphates

KW - Thin films

KW - X ray diffraction analysis

KW - Thin film X ray diffraction

KW - Bone cement

KW - article

KW - chemical analysis

KW - crystal structure

KW - crystallization

KW - immersion

KW - infrared spectroscopy

KW - vibration

KW - X ray diffraction

KW - Biocompatible Materials

KW - Spectroscopy, Fourier Transform Infrared

KW - X-Ray Diffraction

U2 - 10.1002/(SICI)1097-4636(199807)41:1<162::AID-JBM19>3.0.CO;2-P

DO - 10.1002/(SICI)1097-4636(199807)41:1<162::AID-JBM19>3.0.CO;2-P

M3 - Journal article

VL - 41

SP - 162

EP - 166

JO - Journal of Biomedical Materials Research Part A

JF - Journal of Biomedical Materials Research Part A

SN - 0021-9304

IS - 1

ER -

Research

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