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Characterisation of nanocrystalline magnesium oxide by X-ray absorption spectroscopy

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Characterisation of nanocrystalline magnesium oxide by X-ray absorption spectroscopy. / Savin, Shelley L. P.; Chadwick, Alan V.; O'Dell, Luke A. et al.
In: ChemPhysChem, Vol. 8, No. 6, 01.04.2007, p. 882-889.

Research output: Contribution to Journal/MagazineJournal articlepeer-review

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Savin SLP, Chadwick AV, O'Dell LA, Smith ME. Characterisation of nanocrystalline magnesium oxide by X-ray absorption spectroscopy. ChemPhysChem. 2007 Apr 1;8(6):882-889. doi: 10.1002/cphc.200600750

Author

Savin, Shelley L. P. ; Chadwick, Alan V. ; O'Dell, Luke A. et al. / Characterisation of nanocrystalline magnesium oxide by X-ray absorption spectroscopy. In: ChemPhysChem. 2007 ; Vol. 8, No. 6. pp. 882-889.

Bibtex

@article{e86456f98fd746e19ea9f95abe03b397,
title = "Characterisation of nanocrystalline magnesium oxide by X-ray absorption spectroscopy",
abstract = "27Al MAS NMR has been used to study a sol?gel prepared alumina annealed at various temperatures. Two-field simulation of the sample heated to 1200 ?C confirmed the presence of corundum, as suggested by XRD, and also the presence of nanocrystalline theta-Al2O3. 27Al MAS NMR chemical shifts, quadrupolar coupling constants and asymmetry parameters are reported for the tetrahedral and octahedral aluminium sites within theta-Al2O3.",
keywords = "ball-milling, EXAFS spectroscopy, nanocrystalline oxides, sol-gel processes",
author = "Savin, {Shelley L. P.} and Chadwick, {Alan V.} and O'Dell, {Luke A.} and Smith, {Mark E.}",
year = "2007",
month = apr,
day = "1",
doi = "10.1002/cphc.200600750",
language = "English",
volume = "8",
pages = "882--889",
journal = "ChemPhysChem",
issn = "1439-7641",
publisher = "WILEY-V C H VERLAG GMBH",
number = "6",

}

RIS

TY - JOUR

T1 - Characterisation of nanocrystalline magnesium oxide by X-ray absorption spectroscopy

AU - Savin, Shelley L. P.

AU - Chadwick, Alan V.

AU - O'Dell, Luke A.

AU - Smith, Mark E.

PY - 2007/4/1

Y1 - 2007/4/1

N2 - 27Al MAS NMR has been used to study a sol?gel prepared alumina annealed at various temperatures. Two-field simulation of the sample heated to 1200 ?C confirmed the presence of corundum, as suggested by XRD, and also the presence of nanocrystalline theta-Al2O3. 27Al MAS NMR chemical shifts, quadrupolar coupling constants and asymmetry parameters are reported for the tetrahedral and octahedral aluminium sites within theta-Al2O3.

AB - 27Al MAS NMR has been used to study a sol?gel prepared alumina annealed at various temperatures. Two-field simulation of the sample heated to 1200 ?C confirmed the presence of corundum, as suggested by XRD, and also the presence of nanocrystalline theta-Al2O3. 27Al MAS NMR chemical shifts, quadrupolar coupling constants and asymmetry parameters are reported for the tetrahedral and octahedral aluminium sites within theta-Al2O3.

KW - ball-milling, EXAFS spectroscopy, nanocrystalline oxides, sol-gel processes

U2 - 10.1002/cphc.200600750

DO - 10.1002/cphc.200600750

M3 - Journal article

VL - 8

SP - 882

EP - 889

JO - ChemPhysChem

JF - ChemPhysChem

SN - 1439-7641

IS - 6

ER -