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Elucidation of quadrupole parameters by simulation of 10B NMR powder patterns

Research output: Contribution to Journal/Magazine › Journal article › peer-review

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Elucidation of quadrupole parameters by simulation of 10B NMR powder patterns. / Berkowitz, J.; McConnell, M.R.; Tholen, K. et al.
In: Physics and Chemistry of Glasses - European Journal of Glass Science and Technology Part B, Vol. 50, No. 6, 12.2009, p. 372-377.

Research output: Contribution to Journal/Magazine › Journal article › peer-review

Harvard

Berkowitz, J, McConnell, MR, Tholen, K, Feller, S, Affatigato, M, Martin, SW, Holland, D, Smith, ME & Kemp, TF 2009, 'Elucidation of quadrupole parameters by simulation of 10B NMR powder patterns', Physics and Chemistry of Glasses - European Journal of Glass Science and Technology Part B, vol. 50, no. 6, pp. 372-377. <https://www.ingentaconnect.com/content/sgt/ejgst/2009/00000050/00000006/art00007>

APA

Berkowitz, J., McConnell, M. R., Tholen, K., Feller, S., Affatigato, M., Martin, S. W., Holland, D., Smith, M. E., & Kemp, T. F. (2009). Elucidation of quadrupole parameters by simulation of 10B NMR powder patterns. Physics and Chemistry of Glasses - European Journal of Glass Science and Technology Part B, 50(6), 372-377. https://www.ingentaconnect.com/content/sgt/ejgst/2009/00000050/00000006/art00007

Vancouver

Berkowitz J, McConnell MR, Tholen K, Feller S, Affatigato M, Martin SW et al. Elucidation of quadrupole parameters by simulation of 10B NMR powder patterns. Physics and Chemistry of Glasses - European Journal of Glass Science and Technology Part B. 2009 Dec;50(6):372-377.

Author

Berkowitz, J. ; McConnell, M.R. ; Tholen, K. et al. / Elucidation of quadrupole parameters by simulation of 10B NMR powder patterns. In: Physics and Chemistry of Glasses - European Journal of Glass Science and Technology Part B. 2009 ; Vol. 50, No. 6. pp. 372-377.

Bibtex

@article{e460cc25a3dc47bb91f3109fa54984ff,
title = "Elucidation of quadrupole parameters by simulation of 10B NMR powder patterns",
abstract = "A method has been developed to analyse static 10B NMR spectra and, using exhaustive simulation procedures, we have obtained values for quadrupole parameters and their distribution. Experimental data for vitreous boron oxide, vitreous and crystalline caesium triborate, vitreous caesium diborate, crystalline potassium diborate, and caesium enneaborate have been fitted to yield information on the multiple sites and their quadrupole parameters. These sites may result from differences in short range order, or intermediate range structure. The asymmetry parameter is particularly sensitive to differences in the environments of three-coordinated borons placed in differing intermediate range order positions.",
keywords = "Asymmetry parameter, Exhaustive simulation, Experimental data, Intermediate range order, NMR spectrum, Powder patterns, Quadrupoles, Short range orders, Vitreous boron oxide, Amorphous materials, Boron, Boron compounds, Crystalline materials, Nuclear magnetic resonance spectroscopy, Potassium, Cesium",
author = "J. Berkowitz and M.R. McConnell and K. Tholen and S. Feller and M. Affatigato and S.W. Martin and D. Holland and M.E. Smith and T.F. Kemp",
year = "2009",
month = dec,
language = "English",
volume = "50",
pages = "372--377",
journal = "Physics and Chemistry of Glasses - European Journal of Glass Science and Technology Part B",
issn = "1753-3562",
publisher = "Society of Glass Technology",
number = "6",

}

RIS

TY - JOUR

T1 - Elucidation of quadrupole parameters by simulation of 10B NMR powder patterns

AU - Berkowitz, J.

AU - McConnell, M.R.

AU - Tholen, K.

AU - Feller, S.

AU - Affatigato, M.

AU - Martin, S.W.

AU - Holland, D.

AU - Smith, M.E.

AU - Kemp, T.F.

PY - 2009/12

Y1 - 2009/12

N2 - A method has been developed to analyse static 10B NMR spectra and, using exhaustive simulation procedures, we have obtained values for quadrupole parameters and their distribution. Experimental data for vitreous boron oxide, vitreous and crystalline caesium triborate, vitreous caesium diborate, crystalline potassium diborate, and caesium enneaborate have been fitted to yield information on the multiple sites and their quadrupole parameters. These sites may result from differences in short range order, or intermediate range structure. The asymmetry parameter is particularly sensitive to differences in the environments of three-coordinated borons placed in differing intermediate range order positions.

AB - A method has been developed to analyse static 10B NMR spectra and, using exhaustive simulation procedures, we have obtained values for quadrupole parameters and their distribution. Experimental data for vitreous boron oxide, vitreous and crystalline caesium triborate, vitreous caesium diborate, crystalline potassium diborate, and caesium enneaborate have been fitted to yield information on the multiple sites and their quadrupole parameters. These sites may result from differences in short range order, or intermediate range structure. The asymmetry parameter is particularly sensitive to differences in the environments of three-coordinated borons placed in differing intermediate range order positions.

KW - Asymmetry parameter

KW - Exhaustive simulation

KW - Experimental data

KW - Intermediate range order

KW - NMR spectrum

KW - Powder patterns

KW - Quadrupoles

KW - Short range orders

KW - Vitreous boron oxide

KW - Amorphous materials

KW - Boron

KW - Boron compounds

KW - Crystalline materials

KW - Nuclear magnetic resonance spectroscopy

KW - Potassium

KW - Cesium

M3 - Journal article

VL - 50

SP - 372

EP - 377

JO - Physics and Chemistry of Glasses - European Journal of Glass Science and Technology Part B

JF - Physics and Chemistry of Glasses - European Journal of Glass Science and Technology Part B

SN - 1753-3562

IS - 6

ER -