Rights statement: http://journals.cambridge.org/action/displayJournal?jid=JMR The final, definitive version of this article has been published in the Journal, Journal of Materials Research, 26 (18), pp 2355-2368 2011, © 2011 Cambridge University Press.
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Research output: Contribution to Journal/Magazine › Journal article › peer-review
Research output: Contribution to Journal/Magazine › Journal article › peer-review
}
TY - JOUR
T1 - High-resolution solid state NMR experiments for the characterization of calcium phosphate biomaterials and biominerals
AU - Pourpoint, Frédérique
AU - Coelho Diogo, Cristina
AU - Gervais, Christel
AU - Bonhomme, Christian
AU - Fayon, Franck
AU - Laurencin-Dalicieux , Sara
AU - Gennero, Isabelle
AU - Salles, Jean-Pierre
AU - Howes, Andrew P.
AU - Dupree, Ray
AU - Hanna, John V.
AU - Smith, Mark E.
AU - Mauri, Francesco
AU - Guerrero, Gilles
AU - Mutin, P. Hubert
AU - Laurencin, Danielle
N1 - http://journals.cambridge.org/action/displayJournal?jid=JMR The final, definitive version of this article has been published in the Journal, Journal of Materials Research, 26 (18), pp 2355-2368 2011, © 2011 Cambridge University Press.
PY - 2011/9/28
Y1 - 2011/9/28
N2 - Calcium phosphates form a vast family of biominerals, which have attracted much attention in fields like biology, medicine, and materials science, to name a few. Solid state Nuclear Magnetic Resonance (NMR) is one of the few techniques capable of providing information about their structure at the atomic level. Here, examples of recent advances of solid state NMR techniques are given to demonstrate their suitability to characterize in detail synthetic and biological calcium phosphates. Examples of high-resolution 31P, 1H (and 17O), solid state NMR experiments of a 17O-enriched monocalcium phosphate monohydrate-monetite mixture and of a mouse tooth are presented. In both cases, the advantage of performing fast Magic Angle Spinning NMR experiments at high magnetic fields is emphasized, notably because it allows very small volumes of sample to be analyzed.
AB - Calcium phosphates form a vast family of biominerals, which have attracted much attention in fields like biology, medicine, and materials science, to name a few. Solid state Nuclear Magnetic Resonance (NMR) is one of the few techniques capable of providing information about their structure at the atomic level. Here, examples of recent advances of solid state NMR techniques are given to demonstrate their suitability to characterize in detail synthetic and biological calcium phosphates. Examples of high-resolution 31P, 1H (and 17O), solid state NMR experiments of a 17O-enriched monocalcium phosphate monohydrate-monetite mixture and of a mouse tooth are presented. In both cases, the advantage of performing fast Magic Angle Spinning NMR experiments at high magnetic fields is emphasized, notably because it allows very small volumes of sample to be analyzed.
KW - Biomaterial
KW - Nuclear magnetic resonance
KW - Bone
U2 - 10.1557/jmr.2011.250
DO - 10.1557/jmr.2011.250
M3 - Journal article
VL - 26
SP - 2355
EP - 2368
JO - Journal of Materials Research
JF - Journal of Materials Research
SN - 2044-5326
IS - 18
ER -