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In situ high-energy X-ray diffraction study of a bioactive calcium silicate foam immersed in simulated body fluid

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In situ high-energy X-ray diffraction study of a bioactive calcium silicate foam immersed in simulated body fluid. / FitzGerald, V.; Drake, K. O.; Jones, J. R. et al.
In: Journal of Synchrotron Radiation, Vol. 14, No. 6, 01.11.2007, p. 492-499.

Research output: Contribution to Journal/Magazine › Journal article › peer-review

Harvard

FitzGerald, V, Drake, KO, Jones, JR, Smith, ME, Honkimaeki, V, Buslaps, T, Kretzschmer, M & Newport, RJ 2007, 'In situ high-energy X-ray diffraction study of a bioactive calcium silicate foam immersed in simulated body fluid', Journal of Synchrotron Radiation, vol. 14, no. 6, pp. 492-499. https://doi.org/10.1107/S0909049507042173

APA

FitzGerald, V., Drake, K. O., Jones, J. R., Smith, M. E., Honkimaeki, V., Buslaps, T., Kretzschmer, M., & Newport, R. J. (2007). In situ high-energy X-ray diffraction study of a bioactive calcium silicate foam immersed in simulated body fluid. Journal of Synchrotron Radiation, 14(6), 492-499. https://doi.org/10.1107/S0909049507042173

Vancouver

FitzGerald V, Drake KO, Jones JR, Smith ME, Honkimaeki V, Buslaps T et al. In situ high-energy X-ray diffraction study of a bioactive calcium silicate foam immersed in simulated body fluid. Journal of Synchrotron Radiation. 2007 Nov 1;14(6):492-499. doi: 10.1107/S0909049507042173

Author

FitzGerald, V. ; Drake, K. O. ; Jones, J. R. et al. / In situ high-energy X-ray diffraction study of a bioactive calcium silicate foam immersed in simulated body fluid. In: Journal of Synchrotron Radiation. 2007 ; Vol. 14, No. 6. pp. 492-499.

Bibtex

@article{b294132072cf4cfb957f178da646c063,
title = "In situ high-energy X-ray diffraction study of a bioactive calcium silicate foam immersed in simulated body fluid",
abstract = "The method of in situ time-resolved high-energy X-ray diffraction, using the intrinsically highly collimated X-ray beam generated by the European Synchrotron Radiation Facility, is demonstrated. A specially designed cell, which allows the addition of liquid components, has been used to study the reaction mechanisms of a foamed bioactive calcia-silica sol-gel glass immersed in simulated body fluid. Analysis of the X-ray diffraction data from this experiment provides atomic distances, via the pair correlation functions, at different stages of the dissolution of the glass and of the associated calcium phosphate, and ultimately hydroxyapatite, i.e. bone mineral, formation. Hence, changes in the atomic scale structure can be analysed as a function of reaction time, giving an insight into the evolution of the structure of both the glass matrix and the hydroxyapatite surface growth.",
keywords = "high-energy X-ray diffraction, glass structure, bioactive glass, in situ diffraction",
author = "V. FitzGerald and Drake, {K. O.} and Jones, {J. R.} and Smith, {Mark E.} and V. Honkimaeki and T. Buslaps and M. Kretzschmer and Newport, {R. J.}",
year = "2007",
month = nov,
day = "1",
doi = "10.1107/S0909049507042173",
language = "English",
volume = "14",
pages = "492--499",
journal = "Journal of Synchrotron Radiation",
issn = "1600-5775",
publisher = "International Union of Crystallography",
number = "6",

}

RIS

TY - JOUR

T1 - In situ high-energy X-ray diffraction study of a bioactive calcium silicate foam immersed in simulated body fluid

AU - FitzGerald, V.

AU - Drake, K. O.

AU - Jones, J. R.

AU - Smith, Mark E.

AU - Honkimaeki, V.

AU - Buslaps, T.

AU - Kretzschmer, M.

AU - Newport, R. J.

PY - 2007/11/1

Y1 - 2007/11/1

N2 - The method of in situ time-resolved high-energy X-ray diffraction, using the intrinsically highly collimated X-ray beam generated by the European Synchrotron Radiation Facility, is demonstrated. A specially designed cell, which allows the addition of liquid components, has been used to study the reaction mechanisms of a foamed bioactive calcia-silica sol-gel glass immersed in simulated body fluid. Analysis of the X-ray diffraction data from this experiment provides atomic distances, via the pair correlation functions, at different stages of the dissolution of the glass and of the associated calcium phosphate, and ultimately hydroxyapatite, i.e. bone mineral, formation. Hence, changes in the atomic scale structure can be analysed as a function of reaction time, giving an insight into the evolution of the structure of both the glass matrix and the hydroxyapatite surface growth.

AB - The method of in situ time-resolved high-energy X-ray diffraction, using the intrinsically highly collimated X-ray beam generated by the European Synchrotron Radiation Facility, is demonstrated. A specially designed cell, which allows the addition of liquid components, has been used to study the reaction mechanisms of a foamed bioactive calcia-silica sol-gel glass immersed in simulated body fluid. Analysis of the X-ray diffraction data from this experiment provides atomic distances, via the pair correlation functions, at different stages of the dissolution of the glass and of the associated calcium phosphate, and ultimately hydroxyapatite, i.e. bone mineral, formation. Hence, changes in the atomic scale structure can be analysed as a function of reaction time, giving an insight into the evolution of the structure of both the glass matrix and the hydroxyapatite surface growth.

KW - high-energy X-ray diffraction, glass structure, bioactive glass, in situ diffraction

U2 - 10.1107/S0909049507042173

DO - 10.1107/S0909049507042173

M3 - Journal article

VL - 14

SP - 492

EP - 499

JO - Journal of Synchrotron Radiation

JF - Journal of Synchrotron Radiation

SN - 1600-5775

IS - 6

ER -