Home > Research > Publications & Outputs > New insights into the bonding arrangements of L...

Research

Links

Text available via DOI:

View graph of relations

New insights into the bonding arrangements of L- and D-glutamates from solid state 17 O NMR

Research output: Contribution to Journal/Magazine › Journal article › peer-review

Published

Standard

New insights into the bonding arrangements of L- and D-glutamates from solid state 17 O NMR. / Lemaitre, V.; Pike, K.J.; Watts, A. et al.
In: Chemical Physics Letters, Vol. 371, No. 1-2, 28.03.2003, p. 91-97.

Research output: Contribution to Journal/Magazine › Journal article › peer-review

Harvard

Lemaitre, V, Pike, KJ, Watts, A, Anupold, T, Samoson, A, Smith, ME & Dupree, R 2003, 'New insights into the bonding arrangements of L- and D-glutamates from solid state 17 O NMR', Chemical Physics Letters, vol. 371, no. 1-2, pp. 91-97. https://doi.org/10.1016/S0009-2614(03)00254-9

APA

Lemaitre, V., Pike, K. J., Watts, A., Anupold, T., Samoson, A., Smith, M. E., & Dupree, R. (2003). New insights into the bonding arrangements of L- and D-glutamates from solid state 17 O NMR. Chemical Physics Letters, 371(1-2), 91-97. https://doi.org/10.1016/S0009-2614(03)00254-9

Vancouver

Lemaitre V, Pike KJ, Watts A, Anupold T, Samoson A, Smith ME et al. New insights into the bonding arrangements of L- and D-glutamates from solid state 17 O NMR. Chemical Physics Letters. 2003 Mar 28;371(1-2):91-97. doi: 10.1016/S0009-2614(03)00254-9

Author

Lemaitre, V. ; Pike, K.J. ; Watts, A. et al. / New insights into the bonding arrangements of L- and D-glutamates from solid state 17 O NMR. In: Chemical Physics Letters. 2003 ; Vol. 371, No. 1-2. pp. 91-97.

Bibtex

@article{b974236a16f24f4ca8163658eb288ae3,
title = "New insights into the bonding arrangements of L- and D-glutamates from solid state 17 O NMR",
abstract = "Magic angle spinning (MAS) from L- and D-glutamic acid-HCl at 14.1 T produces highly structured and very similar NMR spectra. Lines from all 4 oxygen sites are readily distinguished and assigned. These 17O NMR spectra are very different from the previously reported 17O spectrum of the D,L-form presumably because that was a racemic crystal. 17O NMR from L-monosodium glutamate-HCl is very different again requiring the application of double angle rotation and 3 quantum MAS NMR to provide resolution of 5 different sites. Hence high resolution 17O solid state NMR techniques offer possible new insight into biochemical bonding processes. {\textcopyright} 2003 Elsevier Science B.V. All rights reserved.",
author = "V. Lemaitre and K.J. Pike and A. Watts and T. Anupold and A. Samoson and M.E. Smith and R. Dupree",
year = "2003",
month = mar,
day = "28",
doi = "10.1016/S0009-2614(03)00254-9",
language = "English",
volume = "371",
pages = "91--97",
journal = "Chemical Physics Letters",
issn = "0009-2614",
publisher = "Elsevier",
number = "1-2",

}

RIS

TY - JOUR

T1 - New insights into the bonding arrangements of L- and D-glutamates from solid state 17 O NMR

AU - Lemaitre, V.

AU - Pike, K.J.

AU - Watts, A.

AU - Anupold, T.

AU - Samoson, A.

AU - Smith, M.E.

AU - Dupree, R.

PY - 2003/3/28

Y1 - 2003/3/28

N2 - Magic angle spinning (MAS) from L- and D-glutamic acid-HCl at 14.1 T produces highly structured and very similar NMR spectra. Lines from all 4 oxygen sites are readily distinguished and assigned. These 17O NMR spectra are very different from the previously reported 17O spectrum of the D,L-form presumably because that was a racemic crystal. 17O NMR from L-monosodium glutamate-HCl is very different again requiring the application of double angle rotation and 3 quantum MAS NMR to provide resolution of 5 different sites. Hence high resolution 17O solid state NMR techniques offer possible new insight into biochemical bonding processes. © 2003 Elsevier Science B.V. All rights reserved.

AB - Magic angle spinning (MAS) from L- and D-glutamic acid-HCl at 14.1 T produces highly structured and very similar NMR spectra. Lines from all 4 oxygen sites are readily distinguished and assigned. These 17O NMR spectra are very different from the previously reported 17O spectrum of the D,L-form presumably because that was a racemic crystal. 17O NMR from L-monosodium glutamate-HCl is very different again requiring the application of double angle rotation and 3 quantum MAS NMR to provide resolution of 5 different sites. Hence high resolution 17O solid state NMR techniques offer possible new insight into biochemical bonding processes. © 2003 Elsevier Science B.V. All rights reserved.

U2 - 10.1016/S0009-2614(03)00254-9

DO - 10.1016/S0009-2614(03)00254-9

M3 - Journal article

VL - 371

SP - 91

EP - 97

JO - Chemical Physics Letters

JF - Chemical Physics Letters

SN - 0009-2614

IS - 1-2

ER -