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Sol-gel produced sodium calcium phosphosilicates for bioactive applications: Synthesis and structural characterisation

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Sol-gel produced sodium calcium phosphosilicates for bioactive applications: Synthesis and structural characterisation. / Carta, Daniela; Newport, Robert J.; Knowles, Jonathan C. et al.
In: Materials Chemistry and Physics, Vol. 130, No. 1-2, 2011, p. 690-696.

Research output: Contribution to Journal/Magazine › Journal article › peer-review

Harvard

Carta, D, Newport, RJ, Knowles, JC, Smith, ME & Guerry, P 2011, 'Sol-gel produced sodium calcium phosphosilicates for bioactive applications: Synthesis and structural characterisation', Materials Chemistry and Physics, vol. 130, no. 1-2, pp. 690-696. https://doi.org/10.1016/j.matchemphys.2011.07.050

APA

Carta, D., Newport, R. J., Knowles, J. C., Smith, M. E., & Guerry, P. (2011). Sol-gel produced sodium calcium phosphosilicates for bioactive applications: Synthesis and structural characterisation. Materials Chemistry and Physics, 130(1-2), 690-696. https://doi.org/10.1016/j.matchemphys.2011.07.050

Vancouver

Carta D, Newport RJ, Knowles JC, Smith ME, Guerry P. Sol-gel produced sodium calcium phosphosilicates for bioactive applications: Synthesis and structural characterisation. Materials Chemistry and Physics. 2011;130(1-2):690-696. doi: 10.1016/j.matchemphys.2011.07.050

Author

Carta, Daniela ; Newport, Robert J. ; Knowles, Jonathan C. et al. / Sol-gel produced sodium calcium phosphosilicates for bioactive applications: Synthesis and structural characterisation. In: Materials Chemistry and Physics. 2011 ; Vol. 130, No. 1-2. pp. 690-696.

Bibtex

@article{247fc6b4f3a647979d22f885e78a01de,
title = "Sol-gel produced sodium calcium phosphosilicates for bioactive applications: Synthesis and structural characterisation",
abstract = "A series of phosphosilicates P(2)O(5) (45 mol-CaO (20-40 mol-Na(2)O (5-20 mol-SiO(2) (10-15 mol has been synthesised by the sol-gel route using PO(OH)(3-x)(OC(2)H(5))(x) (x = 1, 2) as the phosphorus precursor. Evolution of the gels with temperature was studied using thermogravimetric analysis and differential thermal analysis. These phosphosilicates show good stability against crystallisation remaining fully amorphous even after calcination at 400 degrees C. The short-range structure of the stabilised sol-gel glasses and the effect of adding modifier oxides to the network structure have been investigated using a combination of techniques: FT-IR spectroscopy, (31)P magic angle spinning NMR, high energy XRD and P L-edge XANES.",
author = "Daniela Carta and Newport, {Robert J.} and Knowles, {Jonathan C.} and Smith, {Mark E.} and Paul Guerry",
year = "2011",
doi = "10.1016/j.matchemphys.2011.07.050",
language = "English",
volume = "130",
pages = "690--696",
journal = "Materials Chemistry and Physics",
publisher = "Elsevier BV",
number = "1-2",

}

RIS

TY - JOUR

T1 - Sol-gel produced sodium calcium phosphosilicates for bioactive applications: Synthesis and structural characterisation

AU - Carta, Daniela

AU - Newport, Robert J.

AU - Knowles, Jonathan C.

AU - Smith, Mark E.

AU - Guerry, Paul

PY - 2011

Y1 - 2011

N2 - A series of phosphosilicates P(2)O(5) (45 mol-CaO (20-40 mol-Na(2)O (5-20 mol-SiO(2) (10-15 mol has been synthesised by the sol-gel route using PO(OH)(3-x)(OC(2)H(5))(x) (x = 1, 2) as the phosphorus precursor. Evolution of the gels with temperature was studied using thermogravimetric analysis and differential thermal analysis. These phosphosilicates show good stability against crystallisation remaining fully amorphous even after calcination at 400 degrees C. The short-range structure of the stabilised sol-gel glasses and the effect of adding modifier oxides to the network structure have been investigated using a combination of techniques: FT-IR spectroscopy, (31)P magic angle spinning NMR, high energy XRD and P L-edge XANES.

AB - A series of phosphosilicates P(2)O(5) (45 mol-CaO (20-40 mol-Na(2)O (5-20 mol-SiO(2) (10-15 mol has been synthesised by the sol-gel route using PO(OH)(3-x)(OC(2)H(5))(x) (x = 1, 2) as the phosphorus precursor. Evolution of the gels with temperature was studied using thermogravimetric analysis and differential thermal analysis. These phosphosilicates show good stability against crystallisation remaining fully amorphous even after calcination at 400 degrees C. The short-range structure of the stabilised sol-gel glasses and the effect of adding modifier oxides to the network structure have been investigated using a combination of techniques: FT-IR spectroscopy, (31)P magic angle spinning NMR, high energy XRD and P L-edge XANES.

U2 - 10.1016/j.matchemphys.2011.07.050

DO - 10.1016/j.matchemphys.2011.07.050

M3 - Journal article

VL - 130

SP - 690

EP - 696

JO - Materials Chemistry and Physics

JF - Materials Chemistry and Physics

IS - 1-2

ER -