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Synthesis and characterization of polymer-based coatings modified with bioactive ceramic and bovine serum albumin

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Synthesis and characterization of polymer-based coatings modified with bioactive ceramic and bovine serum albumin. / Florkiewicz, Wioletta; Slota, Dagmara; Placek, Angelika; Pluta, Klaudia; Tyliszczak, Bozena; Douglas, Timothy; Sobczak-Kupiec, Agnieszka.

In: Journal of Functional Biomaterials, Vol. 12, No. 2, 21, 30.03.2021.

Research output: Contribution to Journal/MagazineJournal articlepeer-review

Harvard

Florkiewicz, W, Slota, D, Placek, A, Pluta, K, Tyliszczak, B, Douglas, T & Sobczak-Kupiec, A 2021, 'Synthesis and characterization of polymer-based coatings modified with bioactive ceramic and bovine serum albumin', Journal of Functional Biomaterials, vol. 12, no. 2, 21. https://doi.org/10.3390/jfb12020021

APA

Florkiewicz, W., Slota, D., Placek, A., Pluta, K., Tyliszczak, B., Douglas, T., & Sobczak-Kupiec, A. (2021). Synthesis and characterization of polymer-based coatings modified with bioactive ceramic and bovine serum albumin. Journal of Functional Biomaterials, 12(2), [21]. https://doi.org/10.3390/jfb12020021

Vancouver

Florkiewicz W, Slota D, Placek A, Pluta K, Tyliszczak B, Douglas T et al. Synthesis and characterization of polymer-based coatings modified with bioactive ceramic and bovine serum albumin. Journal of Functional Biomaterials. 2021 Mar 30;12(2). 21. https://doi.org/10.3390/jfb12020021

Author

Florkiewicz, Wioletta ; Slota, Dagmara ; Placek, Angelika ; Pluta, Klaudia ; Tyliszczak, Bozena ; Douglas, Timothy ; Sobczak-Kupiec, Agnieszka. / Synthesis and characterization of polymer-based coatings modified with bioactive ceramic and bovine serum albumin. In: Journal of Functional Biomaterials. 2021 ; Vol. 12, No. 2.

Bibtex

@article{5a382c70860e4674a78c1f24359ab2eb,
title = "Synthesis and characterization of polymer-based coatings modified with bioactive ceramic and bovine serum albumin",
abstract = "This study involves the synthesis of hydroxyapatite and describes the preparation and characterization of polymer coatings based on poly(ethylene glycol) diacrylate and poly(ethylene glycol) and modified with bovine serum albumin and hydroxyapatite. Hydroxyapatite was obtained by wet chemical synthesis and characterized by X-ray diffraction and FTIR spectroscopy, and its Ca/P molar ratio was determined (1.69 ± 0.08). The ceramic and bovine serum albumin were used in the preparation of composite materials with the polymeric matrix. The chemical composition of coatings was characterized with FTIR spectroscopy, and their morphology was recorded with SEM imaging. Moreover, the measurements of surface roughness parameters and stereometric research were performed. The prepared coatings were subjected to in vitro studies in simulated body fluid and artificial saliva. Changes in chemical composition and morphology after immersion were examined with FTIR spectroscopy and SEM imaging. Based on the conducted research, it can be stated that applied modifiers promote the biomineralization process. The roughness analysis confirmed prepared materials were characterized by the micrometer-scale topography. The materials morphology and roughness, and the morphology of the newly formed apatite deposit, were dependent on the type of the used modifier, and the artificial fluid used in in vitro studies.",
author = "Wioletta Florkiewicz and Dagmara Slota and Angelika Placek and Klaudia Pluta and Bozena Tyliszczak and Timothy Douglas and Agnieszka Sobczak-Kupiec",
year = "2021",
month = mar,
day = "30",
doi = "10.3390/jfb12020021",
language = "English",
volume = "12",
journal = "Journal of Functional Biomaterials",
issn = "2079-4983",
publisher = "Multidisciplinary Digital Publishing Institute (MDPI)",
number = "2",

}

RIS

TY - JOUR

T1 - Synthesis and characterization of polymer-based coatings modified with bioactive ceramic and bovine serum albumin

AU - Florkiewicz, Wioletta

AU - Slota, Dagmara

AU - Placek, Angelika

AU - Pluta, Klaudia

AU - Tyliszczak, Bozena

AU - Douglas, Timothy

AU - Sobczak-Kupiec, Agnieszka

PY - 2021/3/30

Y1 - 2021/3/30

N2 - This study involves the synthesis of hydroxyapatite and describes the preparation and characterization of polymer coatings based on poly(ethylene glycol) diacrylate and poly(ethylene glycol) and modified with bovine serum albumin and hydroxyapatite. Hydroxyapatite was obtained by wet chemical synthesis and characterized by X-ray diffraction and FTIR spectroscopy, and its Ca/P molar ratio was determined (1.69 ± 0.08). The ceramic and bovine serum albumin were used in the preparation of composite materials with the polymeric matrix. The chemical composition of coatings was characterized with FTIR spectroscopy, and their morphology was recorded with SEM imaging. Moreover, the measurements of surface roughness parameters and stereometric research were performed. The prepared coatings were subjected to in vitro studies in simulated body fluid and artificial saliva. Changes in chemical composition and morphology after immersion were examined with FTIR spectroscopy and SEM imaging. Based on the conducted research, it can be stated that applied modifiers promote the biomineralization process. The roughness analysis confirmed prepared materials were characterized by the micrometer-scale topography. The materials morphology and roughness, and the morphology of the newly formed apatite deposit, were dependent on the type of the used modifier, and the artificial fluid used in in vitro studies.

AB - This study involves the synthesis of hydroxyapatite and describes the preparation and characterization of polymer coatings based on poly(ethylene glycol) diacrylate and poly(ethylene glycol) and modified with bovine serum albumin and hydroxyapatite. Hydroxyapatite was obtained by wet chemical synthesis and characterized by X-ray diffraction and FTIR spectroscopy, and its Ca/P molar ratio was determined (1.69 ± 0.08). The ceramic and bovine serum albumin were used in the preparation of composite materials with the polymeric matrix. The chemical composition of coatings was characterized with FTIR spectroscopy, and their morphology was recorded with SEM imaging. Moreover, the measurements of surface roughness parameters and stereometric research were performed. The prepared coatings were subjected to in vitro studies in simulated body fluid and artificial saliva. Changes in chemical composition and morphology after immersion were examined with FTIR spectroscopy and SEM imaging. Based on the conducted research, it can be stated that applied modifiers promote the biomineralization process. The roughness analysis confirmed prepared materials were characterized by the micrometer-scale topography. The materials morphology and roughness, and the morphology of the newly formed apatite deposit, were dependent on the type of the used modifier, and the artificial fluid used in in vitro studies.

U2 - 10.3390/jfb12020021

DO - 10.3390/jfb12020021

M3 - Journal article

VL - 12

JO - Journal of Functional Biomaterials

JF - Journal of Functional Biomaterials

SN - 2079-4983

IS - 2

M1 - 21

ER -