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Synthesis of alpha- and beta-FeOOH iron oxide nanoparticles in non-ionic surfactant medium

Research output: Contribution to Journal/Magazine › Journal article › peer-review

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Synthesis of alpha- and beta-FeOOH iron oxide nanoparticles in non-ionic surfactant medium. / Bashir, S.; McCabe, R. W.; Boxall, C. et al.
In: Journal of Nanoparticle Research, Vol. 11, No. 3, 04.2009, p. 701-706.

Research output: Contribution to Journal/Magazine › Journal article › peer-review

Harvard

Bashir, S, McCabe, RW, Boxall, C, Leaver, MS & Mobbs, D 2009, 'Synthesis of alpha- and beta-FeOOH iron oxide nanoparticles in non-ionic surfactant medium', Journal of Nanoparticle Research, vol. 11, no. 3, pp. 701-706. https://doi.org/10.1007/s11051-008-9467-z

APA

Bashir, S., McCabe, R. W., Boxall, C., Leaver, M. S., & Mobbs, D. (2009). Synthesis of alpha- and beta-FeOOH iron oxide nanoparticles in non-ionic surfactant medium. Journal of Nanoparticle Research, 11(3), 701-706. https://doi.org/10.1007/s11051-008-9467-z

Vancouver

Bashir S, McCabe RW, Boxall C, Leaver MS, Mobbs D. Synthesis of alpha- and beta-FeOOH iron oxide nanoparticles in non-ionic surfactant medium. Journal of Nanoparticle Research. 2009 Apr;11(3):701-706. doi: 10.1007/s11051-008-9467-z

Author

Bashir, S. ; McCabe, R. W. ; Boxall, C. et al. / Synthesis of alpha- and beta-FeOOH iron oxide nanoparticles in non-ionic surfactant medium. In: Journal of Nanoparticle Research. 2009 ; Vol. 11, No. 3. pp. 701-706.

Bibtex

@article{29da6f017b8e4424926b31604b5ce6be,
title = "Synthesis of alpha- and beta-FeOOH iron oxide nanoparticles in non-ionic surfactant medium",
abstract = "Forced hydrolysis of Fe(III) ions in acidic media was performed under controlled synthetic conditions to produce alpha- and beta-FeOOH iron oxides. The forced hydrolysis synthesis was carried out, separately, in an aqueous medium and the lamellar lyotropic liquid crystalline phase of a commercial non-ionic surfactant/water system. The FT-IR analyses confirmed formation of alpha- and beta-FeOOH iron oxides in the aqueous and the surfactant media with slight formation of ferrihydrite and haematite. TEM micrographs have shown that particles formed in the lamellar lyotropic phase are smaller than those produced in the aqueous medium with their smallest size dimension being constrained in the nanometre scale with a size ranging between 5 and 100 nm. Particles produced in the nanoscale size appeared to have different optical properties compared to their counterparts produced in the microscale size.",
keywords = "Templating synthesis, Iron oxide nanoparticles, Lyotropic mesophases, NITRATE SOLUTIONS, NANOSIZED PARTICLES, GOETHITE, HEMATITE, PRECIPITATION, ASSEMBLIES, HYDROXIDES, GLYCOL, GAMMA",
author = "S. Bashir and McCabe, {R. W.} and C. Boxall and Leaver, {M. S.} and D. Mobbs",
year = "2009",
month = apr,
doi = "10.1007/s11051-008-9467-z",
language = "English",
volume = "11",
pages = "701--706",
journal = "Journal of Nanoparticle Research",
issn = "1388-0764",
publisher = "Springer Netherlands",
number = "3",

}

RIS

TY - JOUR

T1 - Synthesis of alpha- and beta-FeOOH iron oxide nanoparticles in non-ionic surfactant medium

AU - Bashir, S.

AU - McCabe, R. W.

AU - Boxall, C.

AU - Leaver, M. S.

AU - Mobbs, D.

PY - 2009/4

Y1 - 2009/4

N2 - Forced hydrolysis of Fe(III) ions in acidic media was performed under controlled synthetic conditions to produce alpha- and beta-FeOOH iron oxides. The forced hydrolysis synthesis was carried out, separately, in an aqueous medium and the lamellar lyotropic liquid crystalline phase of a commercial non-ionic surfactant/water system. The FT-IR analyses confirmed formation of alpha- and beta-FeOOH iron oxides in the aqueous and the surfactant media with slight formation of ferrihydrite and haematite. TEM micrographs have shown that particles formed in the lamellar lyotropic phase are smaller than those produced in the aqueous medium with their smallest size dimension being constrained in the nanometre scale with a size ranging between 5 and 100 nm. Particles produced in the nanoscale size appeared to have different optical properties compared to their counterparts produced in the microscale size.

AB - Forced hydrolysis of Fe(III) ions in acidic media was performed under controlled synthetic conditions to produce alpha- and beta-FeOOH iron oxides. The forced hydrolysis synthesis was carried out, separately, in an aqueous medium and the lamellar lyotropic liquid crystalline phase of a commercial non-ionic surfactant/water system. The FT-IR analyses confirmed formation of alpha- and beta-FeOOH iron oxides in the aqueous and the surfactant media with slight formation of ferrihydrite and haematite. TEM micrographs have shown that particles formed in the lamellar lyotropic phase are smaller than those produced in the aqueous medium with their smallest size dimension being constrained in the nanometre scale with a size ranging between 5 and 100 nm. Particles produced in the nanoscale size appeared to have different optical properties compared to their counterparts produced in the microscale size.

KW - Templating synthesis

KW - Iron oxide nanoparticles

KW - Lyotropic mesophases

KW - NITRATE SOLUTIONS

KW - NANOSIZED PARTICLES

KW - GOETHITE

KW - HEMATITE

KW - PRECIPITATION

KW - ASSEMBLIES

KW - HYDROXIDES

KW - GLYCOL

KW - GAMMA

U2 - 10.1007/s11051-008-9467-z

DO - 10.1007/s11051-008-9467-z

M3 - Journal article

VL - 11

SP - 701

EP - 706

JO - Journal of Nanoparticle Research

JF - Journal of Nanoparticle Research

SN - 1388-0764

IS - 3

ER -