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High-throughput continuous hydrothermal synthesis of an entire nanoceramic phase diagram

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High-throughput continuous hydrothermal synthesis of an entire nanoceramic phase diagram. / Weng, X.; Cockcroft, J.K.; Hyett, G.; Vickers, M.; Boldrin, P.; Tang, C.C.; Thompson, S.P.; Parker, J.E.; Knowles, J.C.; Rehman, I.; Parkin, I.; Evans, J.R.G.; Darr, J.A.

In: Journal of Combinatorial Chemistry, Vol. 11, No. 5, 2009, p. 829-834.

Research output: Contribution to journalJournal articlepeer-review

Harvard

Weng, X, Cockcroft, JK, Hyett, G, Vickers, M, Boldrin, P, Tang, CC, Thompson, SP, Parker, JE, Knowles, JC, Rehman, I, Parkin, I, Evans, JRG & Darr, JA 2009, 'High-throughput continuous hydrothermal synthesis of an entire nanoceramic phase diagram', Journal of Combinatorial Chemistry, vol. 11, no. 5, pp. 829-834. https://doi.org/10.1021/cc900041a

APA

Weng, X., Cockcroft, J. K., Hyett, G., Vickers, M., Boldrin, P., Tang, C. C., Thompson, S. P., Parker, J. E., Knowles, J. C., Rehman, I., Parkin, I., Evans, J. R. G., & Darr, J. A. (2009). High-throughput continuous hydrothermal synthesis of an entire nanoceramic phase diagram. Journal of Combinatorial Chemistry, 11(5), 829-834. https://doi.org/10.1021/cc900041a

Vancouver

Weng X, Cockcroft JK, Hyett G, Vickers M, Boldrin P, Tang CC et al. High-throughput continuous hydrothermal synthesis of an entire nanoceramic phase diagram. Journal of Combinatorial Chemistry. 2009;11(5):829-834. https://doi.org/10.1021/cc900041a

Author

Weng, X. ; Cockcroft, J.K. ; Hyett, G. ; Vickers, M. ; Boldrin, P. ; Tang, C.C. ; Thompson, S.P. ; Parker, J.E. ; Knowles, J.C. ; Rehman, I. ; Parkin, I. ; Evans, J.R.G. ; Darr, J.A. / High-throughput continuous hydrothermal synthesis of an entire nanoceramic phase diagram. In: Journal of Combinatorial Chemistry. 2009 ; Vol. 11, No. 5. pp. 829-834.

Bibtex

@article{e0791c87ed0a4932882f546d2b0af2d9,
title = "High-throughput continuous hydrothermal synthesis of an entire nanoceramic phase diagram",
abstract = "A novel High-Throughput Continuous Hydrothermal (HiTCH) flow synthesis reactor was used to make directly and rapidly a 66-sample nanoparticle library (entire phase diagram) of nanocrystalline CexZryY zO2-δ in less than 12 h. High resolution PXRD data were obtained for the entire heat-treated library (at 1000 °C/1 h) in less than a day using the new robotic beamline 111, located at Diamond Light Source (DLS). This allowed Rietveld-quality powder X-ray diffraction (PXRD) data collection of the entire 66-sample library in < 1 day. Consequently, the authors rapidly mapped out phase behavior and sintering behaviors for the entire library. Out of the entire 66-sample heat-treated library, the PXRD data suggests that 43 possess the fluorite structure, of which 30 (out of 36) are ternary compositions. The speed, quantity and quality of data obtained by our new approach, offers an exciting new development which will allow structure-property relationships to be accessed for nanoceramics in much shorter time periods. {\textcopyright} 2009 American Chemical Society.",
keywords = "nanomaterial, article, ceramics, chemistry, combinatorial chemistry, structure activity relation, synthesis, transmission electron microscopy, X ray crystallography, Ceramics, Combinatorial Chemistry Techniques, Crystallography, X-Ray, Microscopy, Electron, Transmission, Nanostructures, Structure-Activity Relationship",
author = "X. Weng and J.K. Cockcroft and G. Hyett and M. Vickers and P. Boldrin and C.C. Tang and S.P. Thompson and J.E. Parker and J.C. Knowles and I. Rehman and I. Parkin and J.R.G. Evans and J.A. Darr",
year = "2009",
doi = "10.1021/cc900041a",
language = "English",
volume = "11",
pages = "829--834",
journal = "Journal of Combinatorial Chemistry",
issn = "1520-4766",
publisher = "American Chemical Society",
number = "5",

}

RIS

TY - JOUR

T1 - High-throughput continuous hydrothermal synthesis of an entire nanoceramic phase diagram

AU - Weng, X.

AU - Cockcroft, J.K.

AU - Hyett, G.

AU - Vickers, M.

AU - Boldrin, P.

AU - Tang, C.C.

AU - Thompson, S.P.

AU - Parker, J.E.

AU - Knowles, J.C.

AU - Rehman, I.

AU - Parkin, I.

AU - Evans, J.R.G.

AU - Darr, J.A.

PY - 2009

Y1 - 2009

N2 - A novel High-Throughput Continuous Hydrothermal (HiTCH) flow synthesis reactor was used to make directly and rapidly a 66-sample nanoparticle library (entire phase diagram) of nanocrystalline CexZryY zO2-δ in less than 12 h. High resolution PXRD data were obtained for the entire heat-treated library (at 1000 °C/1 h) in less than a day using the new robotic beamline 111, located at Diamond Light Source (DLS). This allowed Rietveld-quality powder X-ray diffraction (PXRD) data collection of the entire 66-sample library in < 1 day. Consequently, the authors rapidly mapped out phase behavior and sintering behaviors for the entire library. Out of the entire 66-sample heat-treated library, the PXRD data suggests that 43 possess the fluorite structure, of which 30 (out of 36) are ternary compositions. The speed, quantity and quality of data obtained by our new approach, offers an exciting new development which will allow structure-property relationships to be accessed for nanoceramics in much shorter time periods. © 2009 American Chemical Society.

AB - A novel High-Throughput Continuous Hydrothermal (HiTCH) flow synthesis reactor was used to make directly and rapidly a 66-sample nanoparticle library (entire phase diagram) of nanocrystalline CexZryY zO2-δ in less than 12 h. High resolution PXRD data were obtained for the entire heat-treated library (at 1000 °C/1 h) in less than a day using the new robotic beamline 111, located at Diamond Light Source (DLS). This allowed Rietveld-quality powder X-ray diffraction (PXRD) data collection of the entire 66-sample library in < 1 day. Consequently, the authors rapidly mapped out phase behavior and sintering behaviors for the entire library. Out of the entire 66-sample heat-treated library, the PXRD data suggests that 43 possess the fluorite structure, of which 30 (out of 36) are ternary compositions. The speed, quantity and quality of data obtained by our new approach, offers an exciting new development which will allow structure-property relationships to be accessed for nanoceramics in much shorter time periods. © 2009 American Chemical Society.

KW - nanomaterial

KW - article

KW - ceramics

KW - chemistry

KW - combinatorial chemistry

KW - structure activity relation

KW - synthesis

KW - transmission electron microscopy

KW - X ray crystallography

KW - Ceramics

KW - Combinatorial Chemistry Techniques

KW - Crystallography, X-Ray

KW - Microscopy, Electron, Transmission

KW - Nanostructures

KW - Structure-Activity Relationship

U2 - 10.1021/cc900041a

DO - 10.1021/cc900041a

M3 - Journal article

VL - 11

SP - 829

EP - 834

JO - Journal of Combinatorial Chemistry

JF - Journal of Combinatorial Chemistry

SN - 1520-4766

IS - 5

ER -