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Residual dipolar couplings by off-magic-angle spinning in solid-state nuclear magnetic resonance Spectroscopy

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  • Giuseppe Pileio
  • Ying Guo
  • Tran N. Pham
  • John M. Griffin
  • Malcolm H. Levitt
  • Steven P. Brown
<mark>Journal publication date</mark>12/09/2007
<mark>Journal</mark>Journal of the American Chemical Society
Issue number36
Number of pages2
Pages (from-to)10972-10973
Publication StatusPublished
Early online date18/08/07
<mark>Original language</mark>English


A solid-state NMR analogue of the solution-state residual dipolar coupling effect is demonstrated. A small misset of the spinning axis by less than 0.5 degrees changes the modulation frequency of spin-echoes, allowing the estimation of internuclear dipole-dipole couplings and hence internuclear distances.