Residual dipolar couplings by off-magic-angle spinning in solid-state nuclear magnetic resonance Spectroscopy

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Residual dipolar couplings by off-magic-angle spinning in solid-state nuclear magnetic resonance Spectroscopy. / Pileio, Giuseppe; Guo, Ying; Pham, Tran N. et al.

In: Journal of the American Chemical Society, Vol. 129, No. 36, 12.09.2007, p. 10972-10973.

Research output: Contribution to Journal/Magazine › Journal article › peer-review

Harvard

Pileio, G, Guo, Y, Pham, TN, Griffin, JM, Levitt, MH & Brown, SP 2007, 'Residual dipolar couplings by off-magic-angle spinning in solid-state nuclear magnetic resonance Spectroscopy', Journal of the American Chemical Society, vol. 129, no. 36, pp. 10972-10973. https://doi.org/10.1021/ja0721115

APA

Pileio, G., Guo, Y., Pham, T. N., Griffin, J. M., Levitt, M. H., & Brown, S. P. (2007). Residual dipolar couplings by off-magic-angle spinning in solid-state nuclear magnetic resonance Spectroscopy. Journal of the American Chemical Society, 129(36), 10972-10973. https://doi.org/10.1021/ja0721115

Vancouver

Pileio G, Guo Y, Pham TN, Griffin JM, Levitt MH, Brown SP. Residual dipolar couplings by off-magic-angle spinning in solid-state nuclear magnetic resonance Spectroscopy. Journal of the American Chemical Society. 2007 Sep 12;129(36):10972-10973. Epub 2007 Aug 18. doi: 10.1021/ja0721115

Author

Pileio, Giuseppe ; Guo, Ying ; Pham, Tran N. et al. / Residual dipolar couplings by off-magic-angle spinning in solid-state nuclear magnetic resonance Spectroscopy. In: Journal of the American Chemical Society. 2007 ; Vol. 129, No. 36. pp. 10972-10973.

Bibtex

@article{c757fc4dc1b842e78c8f037b0603bd00,

title = "Residual dipolar couplings by off-magic-angle spinning in solid-state nuclear magnetic resonance Spectroscopy",

abstract = "A solid-state NMR analogue of the solution-state residual dipolar coupling effect is demonstrated. A small misset of the spinning axis by less than 0.5 degrees changes the modulation frequency of spin-echoes, allowing the estimation of internuclear dipole-dipole couplings and hence internuclear distances.",

keywords = "ROTATING SOLIDS, NMR, DYNAMICS",

author = "Giuseppe Pileio and Ying Guo and Pham, {Tran N.} and Griffin, {John M.} and Levitt, {Malcolm H.} and Brown, {Steven P.}",

year = "2007",

month = sep,

day = "12",

doi = "10.1021/ja0721115",

language = "English",

volume = "129",

pages = "10972--10973",

journal = "Journal of the American Chemical Society",

issn = "0002-7863",

publisher = "AMER CHEMICAL SOC",

number = "36",

}

RIS

TY - JOUR

T1 - Residual dipolar couplings by off-magic-angle spinning in solid-state nuclear magnetic resonance Spectroscopy

AU - Pileio, Giuseppe

AU - Guo, Ying

AU - Pham, Tran N.

AU - Griffin, John M.

AU - Levitt, Malcolm H.

AU - Brown, Steven P.

PY - 2007/9/12

Y1 - 2007/9/12

N2 - A solid-state NMR analogue of the solution-state residual dipolar coupling effect is demonstrated. A small misset of the spinning axis by less than 0.5 degrees changes the modulation frequency of spin-echoes, allowing the estimation of internuclear dipole-dipole couplings and hence internuclear distances.

AB - A solid-state NMR analogue of the solution-state residual dipolar coupling effect is demonstrated. A small misset of the spinning axis by less than 0.5 degrees changes the modulation frequency of spin-echoes, allowing the estimation of internuclear dipole-dipole couplings and hence internuclear distances.

KW - ROTATING SOLIDS

KW - NMR

KW - DYNAMICS

U2 - 10.1021/ja0721115

DO - 10.1021/ja0721115

M3 - Journal article

VL - 129

SP - 10972

EP - 10973

JO - Journal of the American Chemical Society

JF - Journal of the American Chemical Society

SN - 0002-7863

IS - 36

ER -

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