Research output: Contribution to Journal/Magazine › Journal article › peer-review
Residual dipolar couplings by off-magic-angle spinning in solid-state nuclear magnetic resonance Spectroscopy. / Pileio, Giuseppe; Guo, Ying; Pham, Tran N. et al.
In: Journal of the American Chemical Society, Vol. 129, No. 36, 12.09.2007, p. 10972-10973.Research output: Contribution to Journal/Magazine › Journal article › peer-review
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TY - JOUR
T1 - Residual dipolar couplings by off-magic-angle spinning in solid-state nuclear magnetic resonance Spectroscopy
AU - Pileio, Giuseppe
AU - Guo, Ying
AU - Pham, Tran N.
AU - Griffin, John M.
AU - Levitt, Malcolm H.
AU - Brown, Steven P.
PY - 2007/9/12
Y1 - 2007/9/12
N2 - A solid-state NMR analogue of the solution-state residual dipolar coupling effect is demonstrated. A small misset of the spinning axis by less than 0.5 degrees changes the modulation frequency of spin-echoes, allowing the estimation of internuclear dipole-dipole couplings and hence internuclear distances.
AB - A solid-state NMR analogue of the solution-state residual dipolar coupling effect is demonstrated. A small misset of the spinning axis by less than 0.5 degrees changes the modulation frequency of spin-echoes, allowing the estimation of internuclear dipole-dipole couplings and hence internuclear distances.
KW - ROTATING SOLIDS
KW - NMR
KW - DYNAMICS
U2 - 10.1021/ja0721115
DO - 10.1021/ja0721115
M3 - Journal article
VL - 129
SP - 10972
EP - 10973
JO - Journal of the American Chemical Society
JF - Journal of the American Chemical Society
SN - 0002-7863
IS - 36
ER -