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The synthesis and molecular structure of 1-(3,4-dihydroxyphenethyl)-3-hydroxy-2-methylpyridin-4(1H)-one hydrochloride methanol solvate

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Published
  • Steven R. Hall
  • Raymond Roy
  • Dylan T. McLaughlin
  • Kate J. Sullivan
  • Ross C. Barclay
  • Christopher M. Vogels
  • Andreas Decken
  • Stephen A. Westcott
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<mark>Journal publication date</mark>17/05/2013
<mark>Journal</mark>Crystals
Issue number2
Volume3
Number of pages6
Pages (from-to)333-338
Publication StatusPublished
<mark>Original language</mark>English

Abstract

A 3-hydro-4-pyridinone compound derived from maltol and dopamine has been prepared using a microwave reactor. The molecular structure of the protonated product was confirmed by single crystal X-ray diffraction. Crystals were obtained from a saturated solution of methanol and belong to the triclinic space group P-1 with unit cell parameters a = 8.3801(11) Å; b = 9.2583(12) Å; c = 11.5671(15) Å; α = 73.566(2)°; β = 84.514(2)°; γ = 66.578(2)°. The asymmetric unit contains two molecules.