Final published version
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Research output: Contribution to Journal/Magazine › Journal article › peer-review
Research output: Contribution to Journal/Magazine › Journal article › peer-review
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TY - JOUR
T1 - The synthesis and molecular structure of 1-(3,4-dihydroxyphenethyl)-3-hydroxy-2-methylpyridin-4(1H)-one hydrochloride methanol solvate
AU - Hall, Steven R.
AU - Roy, Raymond
AU - McLaughlin, Dylan T.
AU - Sullivan, Kate J.
AU - Barclay, Ross C.
AU - Vogels, Christopher M.
AU - Decken, Andreas
AU - Westcott, Stephen A.
PY - 2013/5/17
Y1 - 2013/5/17
N2 - A 3-hydro-4-pyridinone compound derived from maltol and dopamine has been prepared using a microwave reactor. The molecular structure of the protonated product was confirmed by single crystal X-ray diffraction. Crystals were obtained from a saturated solution of methanol and belong to the triclinic space group P-1 with unit cell parameters a = 8.3801(11) Å; b = 9.2583(12) Å; c = 11.5671(15) Å; α = 73.566(2)°; β = 84.514(2)°; γ = 66.578(2)°. The asymmetric unit contains two molecules.
AB - A 3-hydro-4-pyridinone compound derived from maltol and dopamine has been prepared using a microwave reactor. The molecular structure of the protonated product was confirmed by single crystal X-ray diffraction. Crystals were obtained from a saturated solution of methanol and belong to the triclinic space group P-1 with unit cell parameters a = 8.3801(11) Å; b = 9.2583(12) Å; c = 11.5671(15) Å; α = 73.566(2)°; β = 84.514(2)°; γ = 66.578(2)°. The asymmetric unit contains two molecules.
KW - Dopamine
KW - Hydroxypyridinone
KW - Ligand
KW - X-ray
U2 - 10.3390/cryst3020333
DO - 10.3390/cryst3020333
M3 - Journal article
AN - SCOPUS:84901358069
VL - 3
SP - 333
EP - 338
JO - Crystals
JF - Crystals
SN - 2073-4352
IS - 2
ER -